Toluene-4-sulfonate3-[6-(2-hexadecyloxymethyl-[1,3]dioxolan-4-ylmethoxy)-hexyl]-thiazol-3-ium;

Base Information

Chemical Name:Toluene-4-sulfonate3-[6-(2-hexadecyloxymethyl-[1,3]dioxolan-4-ylmethoxy)-hexyl]-thiazol-3-ium;
CAS No.:131730-37-5
Molecular Formula:C₇H₇O₃S*C₃₀H₅₆NO₄S
Molecular Weight:698.042
Hs Code.:

Synonyms:Toluene-4-sulfonate3-[6-(2-hexadecyloxymethyl-[1,3]dioxolan-4-ylmethoxy)-hexyl]-thiazol-3-ium;

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Chemical Property of Toluene-4-sulfonate3-[6-(2-hexadecyloxymethyl-[1,3]dioxolan-4-ylmethoxy)-hexyl]-thiazol-3-ium;

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Technology Process of Toluene-4-sulfonate3-[6-(2-hexadecyloxymethyl-[1,3]dioxolan-4-ylmethoxy)-hexyl]-thiazol-3-ium;

There total 9 articles about Toluene-4-sulfonate3-[6-(2-hexadecyloxymethyl-[1,3]dioxolan-4-ylmethoxy)-hexyl]-thiazol-3-ium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6145-69-3
3-(hexadecyloxy)-1,2-propanediol

: 131730-37-5
Toluene-4-sulfonate3-[6-(2-hexadecyloxymethyl-[1,3]dioxolan-4-ylmethoxy)-hexyl]-thiazol-3-ium;

Guidance literature:: Multi-step reaction with 7 steps

1: 100 percent / NaIO₄ / acetone; H₂O / 1.5 h / Ambient temperature

2: camphorsulfonic acid (CSA) / toluene / 18 h / Ambient temperature

3: H₂ / 5percent Pd/C / CH₂Cl₂; ethanol / 18 h / 5171.5 Torr / Ambient temperature

4: NaH / dimethylformamide / 4 h / 100 °C

5: camphorsulfonic acid (CSA) / methanol / 16 h / Ambient temperature

6: pyridine / CH₂Cl₂ / 12 h / Ambient temperature

7: Heating

With pyridine; sodium periodate; camphor-10-sulfonic acid; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/jm00105a058

Reference yield:

: 60956-71-0
2-(hexadecyloxy)acetaldehyde

: 131730-37-5
Toluene-4-sulfonate3-[6-(2-hexadecyloxymethyl-[1,3]dioxolan-4-ylmethoxy)-hexyl]-thiazol-3-ium;

Guidance literature:: Multi-step reaction with 6 steps

1: camphorsulfonic acid (CSA) / toluene / 18 h / Ambient temperature

2: H₂ / 5percent Pd/C / CH₂Cl₂; ethanol / 18 h / 5171.5 Torr / Ambient temperature

3: NaH / dimethylformamide / 4 h / 100 °C

4: camphorsulfonic acid (CSA) / methanol / 16 h / Ambient temperature

5: pyridine / CH₂Cl₂ / 12 h / Ambient temperature

6: Heating

With pyridine; camphor-10-sulfonic acid; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jm00105a058

Reference yield:

: 133415-55-1
4-Benzyloxymethyl-2-hexadecyloxymethyl-[1,3]dioxolane

: 131730-37-5
Toluene-4-sulfonate3-[6-(2-hexadecyloxymethyl-[1,3]dioxolan-4-ylmethoxy)-hexyl]-thiazol-3-ium;

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / 5percent Pd/C / CH₂Cl₂; ethanol / 18 h / 5171.5 Torr / Ambient temperature

2: NaH / dimethylformamide / 4 h / 100 °C

3: camphorsulfonic acid (CSA) / methanol / 16 h / Ambient temperature

4: pyridine / CH₂Cl₂ / 12 h / Ambient temperature

5: Heating

With pyridine; camphor-10-sulfonic acid; hydrogen; sodium hydride; palladium on activated charcoal; In methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00105a058