Acetic acid (2S,3R,4R,5S,6R)-5-((2S,3R,4S,5S,6R)-4-acetoxy-6-acetoxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yl ester

Base Information

Chemical Name:Acetic acid (2S,3R,4R,5S,6R)-5-((2S,3R,4S,5S,6R)-4-acetoxy-6-acetoxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yl ester
CAS No.:110425-99-5
Molecular Formula:C₅₄H₅₅NO₁₅
Molecular Weight:958.028
Hs Code.:

Acetic acid (2S,3R,4R,5S,6R)-5-((2S,3R,4S,5S,6R)-4-acetoxy-6-acetoxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yl ester

Synonyms:Acetic acid (2S,3R,4R,5S,6R)-5-((2S,3R,4S,5S,6R)-4-acetoxy-6-acetoxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yl ester

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Chemical Property of Acetic acid (2S,3R,4R,5S,6R)-5-((2S,3R,4S,5S,6R)-4-acetoxy-6-acetoxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yl ester

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Technology Process of Acetic acid (2S,3R,4R,5S,6R)-5-((2S,3R,4S,5S,6R)-4-acetoxy-6-acetoxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yl ester

There total 13 articles about Acetic acid (2S,3R,4R,5S,6R)-5-((2S,3R,4S,5S,6R)-4-acetoxy-6-acetoxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 110425-99-5
Acetic acid (2S,3R,4R,5S,6R)-5-((2S,3R,4S,5S,6R)-4-acetoxy-6-acetoxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yl ester

Guidance literature:: Multi-step reaction with 7 steps

1: NaH / dimethylformamide

2: Zn, acetic acid / tetrahydrofuran

3: pyridine / CH₂Cl₂

4: HBr / CH₂Cl₂

5: Ag silicate, MS₄A / 1,2-dichloro-ethane

6: 1.) Rh(Ph₃P)3Cl; 2.) HgO, HgCl₂ / 1.) EtOH, CH₃CN, H₂O; 2.) aq. acetone

7: pyridine / various solvent(s)

With pyridine; Wilkinson's catalyst; silver silicate; hydrogen bromide; sodium hydride; acetic acid; mercury dichloride; mercury(II) oxide; zinc; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: 89067-88-9
allyl-3,6-di-O-benzyl-2-deoxy-2-N-phthalimido-β-D-glucopyranoside

: 110425-99-5
Acetic acid (2S,3R,4R,5S,6R)-5-((2S,3R,4S,5S,6R)-4-acetoxy-6-acetoxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / AgOTf, MS₄A / 1,2-dichloro-ethane

2: 88 percent / LiOH, 31percent H₂O₂ / tetrahydrofuran; H₂O

3: 94 percent / Ag₂O / KI / dimethylformamide

4: 1.) Rh(Ph₃P)3Cl; 2.) HgO, HgCl₂ / 1.) EtOH, CH₃CN, H₂O; 2.) aq. acetone

5: pyridine / various solvent(s)

With pyridine; lithium hydroxide; Wilkinson's catalyst; dihydrogen peroxide; silver trifluoromethanesulfonate; mercury dichloride; mercury(II) oxide; silver(l) oxide; potassium iodide; In tetrahydrofuran; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;

Reference yield:

: (2R,3S,4S,5R,6R)-4-Allyloxy-2-allyloxymethyl-6-(2,2,2-trichloro-ethoxy)-tetrahydro-pyran-3,5-diol

: 110425-99-5
Acetic acid (2S,3R,4R,5S,6R)-5-((2S,3R,4S,5S,6R)-4-acetoxy-6-acetoxymethyl-3,5-bis-benzyloxy-tetrahydro-pyran-2-yloxy)-4-benzyloxy-6-benzyloxymethyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-tetrahydro-pyran-2-yl ester

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine / various solvent(s)

2: 1.) Zn, AcOH; 2.) SOCl₂ / 2.) DMF / 1.) THF; 2.) CH₂Cl₂

3: 88 percent / AgOTf, MS₄A / 1,2-dichloro-ethane

4: 88 percent / LiOH, 31percent H₂O₂ / tetrahydrofuran; H₂O

5: 94 percent / Ag₂O / KI / dimethylformamide

6: 1.) Rh(Ph₃P)3Cl; 2.) HgO, HgCl₂ / 1.) EtOH, CH₃CN, H₂O; 2.) aq. acetone

7: pyridine / various solvent(s)

With pyridine; lithium hydroxide; Wilkinson's catalyst; thionyl chloride; dihydrogen peroxide; silver trifluoromethanesulfonate; acetic acid; mercury dichloride; mercury(II) oxide; silver(l) oxide; zinc; potassium iodide; In tetrahydrofuran; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;