4-{5-[4-(dihexylamino) phenyl] thiophene-2-yl} 1-methyl pyridinium 4-methylbenzene sulfonate

Base Information

Chemical Name:4-{5-[4-(dihexylamino) phenyl] thiophene-2-yl} 1-methyl pyridinium 4-methylbenzene sulfonate
CAS No.:1236567-79-5
Molecular Formula:C₇H₇O₃S*C₂₈H₃₉N₂S
Molecular Weight:606.894
Hs Code.:

Synonyms:4-{5-[4-(dihexylamino) phenyl] thiophene-2-yl} 1-methyl pyridinium 4-methylbenzene sulfonate

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Chemical Property of 4-{5-[4-(dihexylamino) phenyl] thiophene-2-yl} 1-methyl pyridinium 4-methylbenzene sulfonate

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Technology Process of 4-{5-[4-(dihexylamino) phenyl] thiophene-2-yl} 1-methyl pyridinium 4-methylbenzene sulfonate

There total 4 articles about 4-{5-[4-(dihexylamino) phenyl] thiophene-2-yl} 1-methyl pyridinium 4-methylbenzene sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1236567-70-6
N,N-dihexyl-4-(5-(pyridin-4-yl)thiophene-2-yl)benzenamine

: 80-48-8
methyl p-toluene sulfonate

: 1236567-79-5
4-{5-[4-(dihexylamino) phenyl] thiophene-2-yl} 1-methyl pyridinium 4-methylbenzene sulfonate

Guidance literature:: In dichloromethane; at 20 ℃; for 50h; Cooling with ice;

Reference yield:

: 540-37-4
p-aminoiodobenzene

: 1236567-79-5
4-{5-[4-(dihexylamino) phenyl] thiophene-2-yl} 1-methyl pyridinium 4-methylbenzene sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 22 h / 90 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; methanol / 0.5 h / 70 °C / Inert atmosphere

2.2: 9 h / 70 °C / Inert atmosphere

3.1: dichloromethane / 50 h / 20 °C / Cooling with ice

With sodium carbonate; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 90134-09-1
N,N-dihexyl-4-iodobenzenamine

: 1236567-79-5
4-{5-[4-(dihexylamino) phenyl] thiophene-2-yl} 1-methyl pyridinium 4-methylbenzene sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; methanol / 0.5 h / 70 °C / Inert atmosphere

1.2: 9 h / 70 °C / Inert atmosphere

2.1: dichloromethane / 50 h / 20 °C / Cooling with ice

With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In methanol; dichloromethane; toluene;