C₄₀H₅₈N₂O₇Si

Base Information

Chemical Name:C₄₀H₅₈N₂O₇Si
CAS No.:1264193-96-5
Molecular Formula:C₄₀H₅₈N₂O₇Si
Molecular Weight:706.995
Hs Code.:

C<sub>40</sub>H<sub>58</sub>N<sub>2</sub>O<sub>7</sub>Si

Synonyms:C₄₀H₅₈N₂O₇Si

Suppliers and Price of C₄₀H₅₈N₂O₇Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₀H₅₈N₂O₇Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₀H₅₈N₂O₇Si

There total 8 articles about C₄₀H₅₈N₂O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1264193-81-8
4-{(2R,6R)-4-methylene-6-[(2R,4S,6R)-6-(2-methyloxazol-4-yl)-4-(triisopropylsilanyloxy)tetrahydropyran-2-ylmethyl]tetrahydropyran-2-yl}but-2-ynoic acid phenylamide

: 1264193-96-5
C₄₀H₅₈N₂O₇Si

Guidance literature:: With dmap; In acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol102860r

Reference yield:

: 1264193-78-3
C₁₄H₁₈O₅

: 1264193-96-5
C₄₀H₅₈N₂O₇Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: titanium tetrachloride / dichloromethane / 120 h / -78 - -20 °C / Inert atmosphere

2.1: water; N,N-dimethyl-formamide / 0.17 h / Microwave irradiation; Heating; Sealed tube

3.1: palladium 10% on activated carbon; hydrogen / methanol / 5 h / 20 °C

4.1: phenyllithium / tetrahydrofuran; dibutyl ether / 0 - 20 °C / Inert atmosphere

4.2: 1 h / 20 °C / Inert atmosphere

5.1: pyridine / dichloromethane / 1 h / -5 °C / Inert atmosphere

6.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

6.2: 18 h / -78 - -20 °C / Inert atmosphere

7.1: dmap / acetonitrile / 2 h / 20 °C / Inert atmosphere

With pyridine; dmap; palladium 10% on activated carbon; hydrogen; titanium tetrachloride; phenyllithium; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; dibutyl ether; water; N,N-dimethyl-formamide; acetonitrile; 1.1: Maitland-Japp reaction;
DOI:10.1021/ol102860r

Reference yield:

: C₃₄H₅₁NO₈Si

: 1264193-96-5
C₄₀H₅₈N₂O₇Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: water; N,N-dimethyl-formamide / 0.17 h / Microwave irradiation; Heating; Sealed tube

2.1: palladium 10% on activated carbon; hydrogen / methanol / 5 h / 20 °C

3.1: phenyllithium / tetrahydrofuran; dibutyl ether / 0 - 20 °C / Inert atmosphere

3.2: 1 h / 20 °C / Inert atmosphere

4.1: pyridine / dichloromethane / 1 h / -5 °C / Inert atmosphere

5.1: lithium diisopropyl amide / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

5.2: 18 h / -78 - -20 °C / Inert atmosphere

6.1: dmap / acetonitrile / 2 h / 20 °C / Inert atmosphere

With pyridine; dmap; palladium 10% on activated carbon; hydrogen; phenyllithium; lithium diisopropyl amide; In tetrahydrofuran; methanol; dichloromethane; dibutyl ether; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/ol102860r