5,6,7-trihydroxy-2-[4-[2-(4-morpholinyl)ethoxy]phenyl]-4H-1-benzopyran-4-one

Base Information

Chemical Name:5,6,7-trihydroxy-2-[4-[2-(4-morpholinyl)ethoxy]phenyl]-4H-1-benzopyran-4-one
CAS No.:1436398-09-2
Molecular Formula:C₂₁H₂₁NO₇
Molecular Weight:399.4
Hs Code.:

Synonyms:5,6,7-trihydroxy-2-[4-[2-(4-morpholinyl)ethoxy]phenyl]-4H-1-benzopyran-4-one

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Chemical Property of 5,6,7-trihydroxy-2-[4-[2-(4-morpholinyl)ethoxy]phenyl]-4H-1-benzopyran-4-one

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Technology Process of 5,6,7-trihydroxy-2-[4-[2-(4-morpholinyl)ethoxy]phenyl]-4H-1-benzopyran-4-one

There total 9 articles about 5,6,7-trihydroxy-2-[4-[2-(4-morpholinyl)ethoxy]phenyl]-4H-1-benzopyran-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1619254-65-7
5-hydroxy-6,7-bis(methoxymethoxy)-2-[4-[2-(4-morpholinyl)ethoxy]phenyl]-4H-1-benzopyran-4-one

: 1436398-09-2
5,6,7-trihydroxy-2-[4-[2-(4-morpholinyl)ethoxy]phenyl]-4H-1-benzopyran-4-one

Guidance literature:: With hydrogenchloride; In diethyl ether; dichloromethane; water; at 0 - 25 ℃; for 6h;
DOI:10.2174/1570178611666140421230118

Reference yield:

: 1619254-61-3
5-hydroxy-6,7-bis(methoxymethoxy)-2-[4-(phenylmethoxy)phenyl]-4H-1-benzopyran-4-one

: 1436398-09-2
5,6,7-trihydroxy-2-[4-[2-(4-morpholinyl)ethoxy]phenyl]-4H-1-benzopyran-4-one

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethanol; tetrahydrofuran / 8 h / 760.05 Torr / Inert atmosphere

2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 25 °C / Inert atmosphere

3: hydrogenchloride / water; dichloromethane; diethyl ether / 6 h / 0 - 25 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium iodide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.2174/1570178611666140421230118

Reference yield:

: 529-53-3
scutellarein

: 1436398-09-2
5,6,7-trihydroxy-2-[4-[2-(4-morpholinyl)ethoxy]phenyl]-4H-1-benzopyran-4-one

Guidance literature:: Multi-step reaction with 7 steps

1: diphenylether / 0.5 h / 175 °C / Inert atmosphere

2: potassium carbonate / N,N-dimethyl-formamide / 14 h / 0 - 25 °C / Inert atmosphere

3: acetic acid / water / 1.5 h / Reflux; Inert atmosphere

4: potassium carbonate / acetone / 6 h / Reflux; Inert atmosphere

5: palladium 10% on activated carbon; hydrogen / ethanol; tetrahydrofuran / 8 h / 760.05 Torr / Inert atmosphere

6: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 12 h / 25 °C / Inert atmosphere

7: hydrogenchloride / water; dichloromethane; diethyl ether / 6 h / 0 - 25 °C

With hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; acetic acid; potassium iodide; In tetrahydrofuran; diphenylether; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetone;
DOI:10.2174/1570178611666140421230118