β-4'-O-(2,3,4,6-tetra-acetyl glucosyl) novobiocin

Base Information

Chemical Name:β-4'-O-(2,3,4,6-tetra-acetyl glucosyl) novobiocin
CAS No.:1343473-90-4
Molecular Formula:C₄₅H₅₄N₂O₂₀
Molecular Weight:942.925
Hs Code.:

Synonyms:β-4'-O-(2,3,4,6-tetra-acetyl glucosyl) novobiocin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of β-4'-O-(2,3,4,6-tetra-acetyl glucosyl) novobiocin

Chemical Property:

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Technology Process of β-4'-O-(2,3,4,6-tetra-acetyl glucosyl) novobiocin

There total 4 articles about β-4'-O-(2,3,4,6-tetra-acetyl glucosyl) novobiocin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 303-81-1,107781-69-1
novobiocin

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1343473-90-4
β-4'-O-(2,3,4,6-tetra-acetyl glucosyl) novobiocin

Guidance literature:: mercury(II) cyanide; In tetrahydrofuran; at 0 ℃; for 168h; Molecular sieve;

Reference yield:

: 303-81-1,107781-69-1
novobiocin

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1343473-90-4
β-4'-O-(2,3,4,6-tetra-acetyl glucosyl) novobiocin

: C₄₅H₅₄N₂O₂₀

: C₅₉H₇₂N₂O₂₉

: C₄₅H₅₄N₂O₂₀

Guidance literature:: With benzyl tri-n-butylammonium bromide; potassium carbonate; In tetrahydrofuran; chloroform; at 20 ℃; for 168h; Reagent/catalyst; Solvent; Temperature; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2017.10.011

Reference yield:

: 1476-53-5,6990-02-9,18656-99-0
sodium novobiocin

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 1343473-90-4
β-4'-O-(2,3,4,6-tetra-acetyl glucosyl) novobiocin

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 72h; Solvent; Temperature; regioselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2017.10.011