N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline

Base Information

• Chemical Name: N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline
• CAS No.: 80825-61-2
• Molecular Formula: C₁₀H₉N₅O₈
• Molecular Weight: 327.21
• Mol file: 80825-61-2.mol

Synonyms:N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline

Chemical Property of N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline

There total 3 articles about N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

1,4-bis(acetylnitroamino)-2,3-dinitrobenzene (80825-62-3) → N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline (80825-61-2)

Guidance literature:

With hydrogen sulfide; In chloroform; at 15 ℃; for 1h;

Reference yield:

N,N'-diacetyl-1,4-phenylenediamine (140-50-1) → N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline (80825-61-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / HNO₃ (d 1.51), acetic acid / 3 h / 35 - 40 °C / then 24 h at 0 to 5 deg. C

2: 40 percent / HNO₃ (d 1.51), acetic anhydride / 3 h / 0 °C

With nitric acid; acetic anhydride; acetic acid;

Reference yield:

N,N'-diacetyl-2,3-dinitro-1,4-phenylenediamine (7756-00-5) → N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline (80825-61-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / HNO₃ (d 1.51), acetic anhydride / 3 h / 0 °C

2: 80 percent / H₂S / CHCl₃ / 1 h / 15 °C

With hydrogen sulfide; nitric acid; acetic anhydride; In chloroform;

upstream raw materials:

1,4-bis(acetylnitroamino)-2,3-dinitrobenzene

N,N'-diacetyl-2,3-dinitro-1,4-phenylenediamine

N,N'-diacetyl-1,4-phenylenediamine

Downstream raw materials:

N,N'-diacetyl-2,3-dinitro-1,4-phenylenediamine

potassium salt of N-acetyl-2,3-dinitro-4-nitroaminoaniline

N-acetyl-2,3-dinitro-1,4-phenylenediamine

N-acetyl-2,3-dinitrobenzene-4-nitroaminoaniline