N-(4-acetamido-2,3-dinitrophenyl)acetamide

Base Information

• Chemical Name: N-(4-acetamido-2,3-dinitrophenyl)acetamide
• CAS No.: 7756-00-5
• Molecular Formula: C10H10N4O6
• Molecular Weight: 282.2096
• Hs Code.: 2924299090
• European Community (EC) Number: 654-051-4
• DSSTox Substance ID: DTXSID80398952
• Wikidata: Q82201218
• Mol file: 7756-00-5.mol

Synonyms:7756-00-5;N-(4-acetamido-2,3-dinitrophenyl)acetamide;N,N'-(2,3-Dinitro-1,4-phenylene) bisacetamide;DTXSID80398952;DGNNIDWBARYYSR-UHFFFAOYSA-N;AKOS024319194;FT-0633412;N,N'-(2,3-dinitro-1,4-phenylene)diacetamide;N,N'-(2,3-Dinitro-1,4-phenylene)bisacetamide;N,N'-(2,3-dinitrobenzene-1,4-diyl)diacetamide;N,N'-(2,3-Dinitro-1,4-phenylene)bis-acetamide;Acetamide, N,N'-(2,3-dinitro-1,4-phenylene)bis-;N,N'-(2,3-DINITRO-1,4-PHENYLENE) BIS-ACETAMIDE

Chemical Property of N-(4-acetamido-2,3-dinitrophenyl)acetamide

Chemical Property:

• Melting Point: 254°C
• Refractive Index: 1.6500 (estimate)
• Boiling Point: 585 °C at 760 mmHg
• Flash Point: 307.6 °C
• PSA: 149.84000
• Density: 1.574 g/cm³
• LogP: 2.61220
• XLogP3: 1
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 2
• Exact Mass: 282.06003405
• Heavy Atom Count: 20
• Complexity: 388

Purity/Quality:

99% ^*data from raw suppliers

N,N'-(2,3-DINITRO-1,4-PHENYLENE)BISACETAMIDE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)NC1=C(C(=C(C=C1)NC(=O)C)[N+](=O)[O-])[N+](=O)[O-]

Technology Process of N-(4-acetamido-2,3-dinitrophenyl)acetamide

There total 4 articles about N-(4-acetamido-2,3-dinitrophenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

N,N'-diacetyl-1,4-phenylenediamine (140-50-1) → N,N'-diacetyl-2,3-dinitro-1,4-phenylenediamine (7756-00-5)

Guidance literature:

With nitric acid; acetic anhydride; acetic acid; at 0 - 20 ℃; for 5h;

DOI:10.1002/zaac.201500703

Reference yield: 80.0%

N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline (80825-61-2) → N,N'-diacetyl-2,3-dinitro-1,4-phenylenediamine (7756-00-5)

Guidance literature:

With hydrogen sulfide; In chloroform; at 15 ℃; for 1h;

Reference yield:

1,4-phenylenediamine (106-50-3) → N,N'-diacetyl-2,3-dinitro-1,4-phenylenediamine (7756-00-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 6 h / 90 °C

2: nitric acid; acetic acid; acetic anhydride / 5 h / 0 - 20 °C

With nitric acid; acetic anhydride; acetic acid;

DOI:10.1002/zaac.201500703

upstream raw materials:

N,N'-diacetyl-1,4-phenylenediamine

N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline

1,4-phenylenediamine

Downstream raw materials:

2,3-dinitro-1,4-bis-(4-nitro-benzoylamino)-benzene

1,4-Diacetamido-2-nitro-3-N-pyrrolidinobenzene

N-acetyl-2,3-dinitrobenzene-4-nitroaminoaniline

N,N'-diacetyl-2,3-dinitro-4-nitroaminoaniline