Dibutyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucipyranosyl phosphate

Base Information

Chemical Name:Dibutyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucipyranosyl phosphate
CAS No.:331281-73-3
Molecular Formula:C₄₂H₅₀ClO₁₁P
Molecular Weight:797.279
Hs Code.:

Synonyms:Dibutyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucipyranosyl phosphate

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Chemical Property of Dibutyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucipyranosyl phosphate

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Technology Process of Dibutyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucipyranosyl phosphate

There total 3 articles about Dibutyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucipyranosyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7693-45-0
4-Chlorophenyl chloroformate

: 208656-41-1
Phosphoric acid (2S,3R,4R,5R,6R)-4,5-bis-benzyloxy-6-benzyloxymethyl-3-hydroxy-tetrahydro-pyran-2-yl ester dibutyl ester

: 331281-73-3
Dibutyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucipyranosyl phosphate

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 0.5h;

Reference yield:

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 331281-73-3
Dibutyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucipyranosyl phosphate

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyldioxirane / CH₂Cl₂; acetone / 0.33 h / 0 °C

2: CH₂Cl₂ / 0.17 h / -78 °C

3: 0.663 g / DMAP / CH₂Cl₂ / 0.5 h / 0 - 20 °C

With dmap; 3,3-dimethyldioxirane; In dichloromethane; acetone;

Reference yield:

: 74372-90-0
3,4,6-tri-O-benzyl-D-glucal epoxide

: 331281-73-3
Dibutyl 3,4,6-tri-O-benzyl-2-O-para-chlorophenylcarbonyl-β-D-glucipyranosyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.17 h / -78 °C

2: 0.663 g / DMAP / CH₂Cl₂ / 0.5 h / 0 - 20 °C

With dmap; In dichloromethane;