benzyl (1S,3R)-3-amino-1-isopropylcyclopentanecarboxylate hydrochloride

Base Information

Chemical Name:benzyl (1S,3R)-3-amino-1-isopropylcyclopentanecarboxylate hydrochloride
CAS No.:625126-75-2
Molecular Formula:C₁₆H₂₃NO₂*ClH
Molecular Weight:297.825
Hs Code.:

Synonyms:benzyl (1S,3R)-3-amino-1-isopropylcyclopentanecarboxylate hydrochloride

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Chemical Property of benzyl (1S,3R)-3-amino-1-isopropylcyclopentanecarboxylate hydrochloride

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Technology Process of benzyl (1S,3R)-3-amino-1-isopropylcyclopentanecarboxylate hydrochloride

There total 7 articles about benzyl (1S,3R)-3-amino-1-isopropylcyclopentanecarboxylate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 625126-74-1
C₂₁H₃₁NO₄

: 625126-75-2
benzyl (1S,3R)-3-amino-1-isopropylcyclopentanecarboxylate hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 1 - 2h; Product distribution / selectivity;

Reference yield:

: 75-30-9
2-iodo-propane

: 625098-78-4
benzyl (1S,3R)-3-[(diphenylmethylene)amino]cyclopentanecarboxylate

: C₁₆H₂₃NO₂*ClH

: 625126-75-2
benzyl (1S,3R)-3-amino-1-isopropylcyclopentanecarboxylate hydrochloride

Guidance literature:: benzyl (1S,3R)-3-[(diphenylmethylene)amino]cyclopentanecarboxylate; With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; at -78 ℃; for 0.833333h;

2-iodo-propane; In tetrahydrofuran; n-heptane; at -78 - 0 ℃; for 2.5h;

With hydrogenchloride; water; In tetrahydrofuran; for 1h;

Reference yield:

: 134003-04-6
(1R,4S)-4-aminocyclopenten-2-ene-1-carboxylic acid

: 625126-75-2
benzyl (1S,3R)-3-amino-1-isopropylcyclopentanecarboxylate hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran; water / 0.5 h

1.2: 168 h

1.3: pH 3

2.1: hydrogen / palladium 10% on activated carbon / methanol / 1 h

3.1: potassium carbonate / DMF (N,N-dimethyl-formamide) / 0.33 h

3.2: 3 h / 20 °C

4.1: hydrogenchloride / 1,4-dioxane

5.1: dichloromethane

6.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane / 0.83 h / -78 °C

6.2: 2.5 h / -78 - 0 °C

6.3: 1 h

With hydrogenchloride; hydrogen; sodium hydrogencarbonate; potassium carbonate; lithium diisopropyl amide; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; DMF (N,N-dimethyl-formamide); n-heptane; dichloromethane; water;