6-(3-(4-methoxybenzyloxy)propyl)-3-((Z)-dec-1-enyl)-2,4-dimethylpyridine

Base Information

Chemical Name:6-(3-(4-methoxybenzyloxy)propyl)-3-((Z)-dec-1-enyl)-2,4-dimethylpyridine
CAS No.:1392469-42-9
Molecular Formula:C₂₈H₄₁NO₂
Molecular Weight:423.639
Hs Code.:

Synonyms:6-(3-(4-methoxybenzyloxy)propyl)-3-((Z)-dec-1-enyl)-2,4-dimethylpyridine

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Chemical Property of 6-(3-(4-methoxybenzyloxy)propyl)-3-((Z)-dec-1-enyl)-2,4-dimethylpyridine

Chemical Property:

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Technology Process of 6-(3-(4-methoxybenzyloxy)propyl)-3-((Z)-dec-1-enyl)-2,4-dimethylpyridine

There total 5 articles about 6-(3-(4-methoxybenzyloxy)propyl)-3-((Z)-dec-1-enyl)-2,4-dimethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1333320-20-9
diisopropyl (Z)-1-decenylboronate

: 1392469-41-8
2-(3-(4-methoxybenzyloxy)propyl)-5-bromo-4,6-dimethylpyridine

: 1392469-42-9
6-(3-(4-methoxybenzyloxy)propyl)-3-((Z)-dec-1-enyl)-2,4-dimethylpyridine

Guidance literature:: 2-(3-(4-methoxybenzyloxy)propyl)-5-bromo-4,6-dimethylpyridine; With palladium diacetate; sodium carbonate; triphenylphosphine; In water; toluene; for 0.5h; Inert atmosphere;

diisopropyl (Z)-1-decenylboronate; In ethanol; water; toluene; Inert atmosphere; Reflux;
DOI:10.1016/j.bmcl.2012.05.127

Reference yield:

: 89856-44-0
2-amino-5-bromo-4,6-dimethylpyridine

: 1392469-42-9
6-(3-(4-methoxybenzyloxy)propyl)-3-((Z)-dec-1-enyl)-2,4-dimethylpyridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen bromide; sodium nitrite / water / 0.5 h / 0 - 5 °C

1.2: 0.5 h / 5 °C

2.1: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

3.1: platinum(IV) oxide; hydrogen; triethylamine / ethanol / 3 h

4.1: palladium diacetate; sodium carbonate; triphenylphosphine / water; toluene / 0.5 h / Inert atmosphere

4.2: Inert atmosphere; Reflux

With piperidine; platinum(IV) oxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydrogen bromide; hydrogen; palladium diacetate; sodium carbonate; triethylamine; triphenylphosphine; sodium nitrite; In tetrahydrofuran; ethanol; water; toluene;
DOI:10.1016/j.bmcl.2012.05.127

Reference yield:

: 5006-57-5
3,6-dibromo-2,4-dimethylpyridine

: 1392469-42-9
6-(3-(4-methoxybenzyloxy)propyl)-3-((Z)-dec-1-enyl)-2,4-dimethylpyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2.1: platinum(IV) oxide; hydrogen; triethylamine / ethanol / 3 h

3.1: palladium diacetate; sodium carbonate; triphenylphosphine / water; toluene / 0.5 h / Inert atmosphere

3.2: Inert atmosphere; Reflux

With piperidine; platinum(IV) oxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; hydrogen; palladium diacetate; sodium carbonate; triethylamine; triphenylphosphine; In tetrahydrofuran; ethanol; water; toluene;
DOI:10.1016/j.bmcl.2012.05.127