C₃₄H₃₉F₅N₈O₂Si

Base Information

Chemical Name:C₃₄H₃₉F₅N₈O₂Si
CAS No.:1334303-82-0
Molecular Formula:C₃₄H₃₉F₅N₈O₂Si
Molecular Weight:714.814
Hs Code.:

C<sub>34</sub>H<sub>39</sub>F<sub>5</sub>N<sub>8</sub>O<sub>2</sub>Si

Synonyms:C₃₄H₃₉F₅N₈O₂Si

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Chemical Property of C₃₄H₃₉F₅N₈O₂Si

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Technology Process of C₃₄H₃₉F₅N₈O₂Si

There total 8 articles about C₃₄H₃₉F₅N₈O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 1334303-82-0
C₃₄H₃₉F₅N₈O₂Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C

1.2: 1 h / 0 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 1 h / 110 °C / Inert atmosphere

2.2: 2 h / 20 °C

2.3: pH 9 - 10

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C

4.1: hydrogenchloride / 1,4-dioxane; tetrahydrofuran / 2 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; sodium tris(acetoxy)borohydride / tetrahydrofuran / 2 h / 20 °C

6.1: hydrogenchloride / 1,4-dioxane; tetrahydrofuran / 2 h / 10 - 20 °C

7.1: triethylamine / tetrahydrofuran / 1 h / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; sodium hydride; sodium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 1015610-23-7
5-fluoro-4-iodo-1H-pyrrolo[2,3-b]pyridine

: 1334303-82-0
C₃₄H₃₉F₅N₈O₂Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C

1.2: 1 h / 0 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 1 h / 110 °C / Inert atmosphere

2.2: 2 h / 20 °C

2.3: pH 9 - 10

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C

4.1: hydrogenchloride / 1,4-dioxane; tetrahydrofuran / 2 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; sodium tris(acetoxy)borohydride / tetrahydrofuran / 2 h / 20 °C

6.1: hydrogenchloride / 1,4-dioxane; tetrahydrofuran / 2 h / 10 - 20 °C

7.1: triethylamine / tetrahydrofuran / 1 h / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; sodium hydride; sodium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; water; N,N-dimethyl-formamide; acetonitrile; mineral oil;

Reference yield:

: 1334303-76-2
5-fluoro-4-iodo-1-{[2-(trimethylsilyl)ethoxy]methyl}-1H-pyrrolo[2,3-b]pyridine

: 1334303-82-0
C₃₄H₃₉F₅N₈O₂Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 1 h / 110 °C / Inert atmosphere

1.2: 2 h / 20 °C

1.3: pH 9 - 10

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C

3.1: hydrogenchloride / 1,4-dioxane; tetrahydrofuran / 2 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; sodium tris(acetoxy)borohydride / tetrahydrofuran / 2 h / 20 °C

5.1: hydrogenchloride / 1,4-dioxane; tetrahydrofuran / 2 h / 10 - 20 °C

6.1: triethylamine / tetrahydrofuran / 1 h / 20 °C

With hydrogenchloride; sodium tris(acetoxy)borohydride; sodium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,4-dioxane; water; acetonitrile;