cis-1-methylpiperidine-4,3-acetolactone methiodide

Base Information

Chemical Name:cis-1-methylpiperidine-4,3-acetolactone methiodide
CAS No.:82244-18-6
Molecular Formula:C₉H₁₆NO₂*I
Molecular Weight:297.136
Hs Code.:

Synonyms:cis-1-methylpiperidine-4,3-acetolactone methiodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-1-methylpiperidine-4,3-acetolactone methiodide

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Technology Process of cis-1-methylpiperidine-4,3-acetolactone methiodide

There total 1 articles about cis-1-methylpiperidine-4,3-acetolactone methiodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19099-93-5
benzyl 4-oxo-1-piperidinecarboxylate

: 82244-18-6
cis-1-methylpiperidine-4,3-acetolactone methiodide

Guidance literature:: Multi-step reaction with 7 steps

1: 1.) NaH / 1.) abs. Et₂O; 2.) abs. Et₂O, abs. benzene

2: 84 percent / ethanol / 5.5 h / 22 °C / Irradiation

3: 97 percent / m-chloroperbenzoic acid / CHCl₃

4: 93 percent / 2 N H₂SO₄ / acetone / 6 h / Heating

5: 73 percent / SOCl₂ / pyridine

6: 1.) hydrogen; 2.) NaBH₃CN / 1.) 5percent Pd-C / 1.) MeOH; 2.) MeOH; 2 h

7: 86.9 percent / acetone / 24 h

With thionyl chloride; sulfuric acid; hydrogen; sodium hydride; sodium cyanoborohydride; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In pyridine; ethanol; chloroform; acetone;
DOI:10.1248/cpb.30.1084