azide

Base Information

• Chemical Name: azide
• CAS No.: 24512-97-8
• Molecular Formula: C₁₂H₁₃N₃O₂
• Molecular Weight: 231.254
• Mol file: 24512-97-8.mol

Synonyms:azide

Chemical Property of azide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of azide

There total 2 articles about azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

ethyl-2-azidoacetate (637-81-0) + 2-methylphenyl aldehyde (529-20-4) → azide (24512-97-8)

Guidance literature:

With sodium ethanolate; In ethanol; at -20 - -10 ℃; for 2h;

Reference yield:

→ azide (24512-97-8)

Guidance literature:

DOI:10.1007/BF00900176

Reference yield: 97.0%

azide (24512-97-8) → 4-methyl-1H-indole-2-carboxylic acid ethyl ester (16732-80-2)

Guidance literature:

In toluene; Heating;

DOI:10.1039/c39820000003

upstream raw materials:

ethyl-2-azidoacetate

2-methylphenyl aldehyde

Downstream raw materials:

ethyl isoquinoline-3-carboxylate

4-methyl-1H-indole-2-carboxylic acid ethyl ester

3-o-Tolyl-3H-azirine-2-carboxylic acid ethyl ester

ethyl 4-acetyl-2-(2-methylphenyl)-5-methyl-1H-pyrrole-3-carboxylate