C₃₅H₄₈N₄O₃SSi

Base Information

Chemical Name:C₃₅H₄₈N₄O₃SSi
CAS No.:1322574-66-2
Molecular Formula:C₃₅H₄₈N₄O₃SSi
Molecular Weight:632.943
Hs Code.:

C<sub>35</sub>H<sub>48</sub>N<sub>4</sub>O<sub>3</sub>SSi

Synonyms:C₃₅H₄₈N₄O₃SSi

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Chemical Property of C₃₅H₄₈N₄O₃SSi

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Technology Process of C₃₅H₄₈N₄O₃SSi

There total 7 articles about C₃₅H₄₈N₄O₃SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1322574-48-0
(3S,4R,6S,7S)-7-((tert-butyldiphenylsilyl)oxy)-4-(methoxymethoxy)-3,6-di methyloctan-1-ol

: 86-93-1
1-Phenyl-1H-tetrazole-5-thiol

: 1322574-66-2
C₃₅H₄₈N₄O₃SSi

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃; for 19h; Inert atmosphere;
DOI:10.1016/j.tet.2011.06.025

Reference yield:

: 945903-61-7
(3S,4S)-4-tert-butyldiphenylsilyloxy-3-methyl-pentan-1-al

: 1322574-66-2
C₃₅H₄₈N₄O₃SSi

Guidance literature:: Multi-step reaction with 4 steps

1.1: toluene / 3 h / -78 °C / Inert atmosphere; Molecular sieve

1.2: 2 h / -78 - 20 °C / Inert atmosphere

2.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 0 - 40 °C / Inert atmosphere

3.1: dimethylsulfide borane complex / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere

3.2: 2 h / 0 - 20 °C / Inert atmosphere

4.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 19 h / 0 - 20 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; dimethylsulfide borane complex; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene; 1.1: Roush crotylation / 4.1: Mitsunobu reaction;
DOI:10.1016/j.tet.2011.06.025

Reference yield:

: 1197349-14-6
C₂₄H₃₂O₃Si

: 1322574-66-2
C₃₅H₄₈N₄O₃SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.2: 0.67 h / -78 - 20 °C / Inert atmosphere

3.1: (2R,5R)-(+)-2-tert-butyl-3-methyl-5-benzyl-4-imidazolidinone; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; trifluoroacetic acid / chloroform / 72 h / -30 °C / Inert atmosphere

4.1: toluene / 3 h / -78 °C / Inert atmosphere; Molecular sieve

4.2: 2 h / -78 - 20 °C / Inert atmosphere

5.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / dichloromethane / 24 h / 0 - 40 °C / Inert atmosphere

6.1: dimethylsulfide borane complex / tetrahydrofuran / 6 h / 0 - 20 °C / Inert atmosphere

6.2: 2 h / 0 - 20 °C / Inert atmosphere

7.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 19 h / 0 - 20 °C / Inert atmosphere

With (2R,5R)-(+)-2-tert-butyl-3-methyl-5-benzyl-4-imidazolidinone; oxalyl dichloride; di-isopropyl azodicarboxylate; dimethylsulfide borane complex; diethyl 2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylate; tetra-(n-butyl)ammonium iodide; diisobutylaluminium hydride; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; chloroform; toluene; 2.1: Swern oxidation / 2.2: Swern oxidation / 4.1: Roush crotylation / 7.1: Mitsunobu reaction;
DOI:10.1016/j.tet.2011.06.025