(2'S,5'S,2''S,5''S,1R,4S)-1,4-bis-[N'-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)methyl]-pyrrolidin-2'-yl-4-acetoxy-butan-1-ol

Base Information

Chemical Name:(2'S,5'S,2''S,5''S,1R,4S)-1,4-bis-[N'-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)methyl]-pyrrolidin-2'-yl-4-acetoxy-butan-1-ol
CAS No.:782496-18-8
Molecular Formula:C₅₈H₈₂N₂O₉Si₂
Molecular Weight:1007.47
Hs Code.:

Synonyms:(2'S,5'S,2''S,5''S,1R,4S)-1,4-bis-[N'-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)methyl]-pyrrolidin-2'-yl-4-acetoxy-butan-1-ol

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Chemical Property of (2'S,5'S,2''S,5''S,1R,4S)-1,4-bis-[N'-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)methyl]-pyrrolidin-2'-yl-4-acetoxy-butan-1-ol

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Technology Process of (2'S,5'S,2''S,5''S,1R,4S)-1,4-bis-[N'-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)methyl]-pyrrolidin-2'-yl-4-acetoxy-butan-1-ol

There total 2 articles about (2'S,5'S,2''S,5''S,1R,4S)-1,4-bis-[N'-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)methyl]-pyrrolidin-2'-yl-4-acetoxy-butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 782496-16-6
(2'S,5'S,2''S,5''S,1R,4S)-1,4-bis-[N'-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)methyl]-pyrrolidin-2'-yl-4-acetoxy-2-butyn-1-ol

: 782496-18-8
(2'S,5'S,2''S,5''S,1R,4S)-1,4-bis-[N'-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)methyl]-pyrrolidin-2'-yl-4-acetoxy-butan-1-ol

Guidance literature:: With hydrogen; platinum on activated charcoal; In ethyl acetate; for 16h; under 760 Torr;
DOI:10.1002/chem.200400181

Reference yield:

: 782496-14-4
(2'S,5'S,2''S,5''S,1R,4S)-1,4-bis-[N'-tert-butoxycarbonyl-5'-(tert-butyldiphenylsilyloxy)methyl]-pyrrolidin-2'-yl-1-(trimethylsilyl)oxy-4-acetoxy-2-butyne

: 782496-18-8
(2'S,5'S,2''S,5''S,1R,4S)-1,4-bis-[N'-tert-butoxycarbonyl-5-(tert-butyldiphenylsilyloxy)methyl]-pyrrolidin-2'-yl-4-acetoxy-butan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / CSA / tetrahydrofuran; methanol / 0.25 h / -10 °C

2: 98 percent / H₂ / Pt/C / ethyl acetate / 16 h / 760 Torr

With camphor-10-sulfonic acid; hydrogen; platinum on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate;
DOI:10.1002/chem.200400181