O₂-(acetoxymethyl) 1-{2-[2-[1-(4-chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetoxymethyloxycarbonyl]pyrrolidin-1-yl}diazen-1-ium-1,2-diolate

Base Information

• Chemical Name: O₂-(acetoxymethyl) 1-{2-[2-[1-(4-chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetoxymethyloxycarbonyl]pyrrolidin-1-yl}diazen-1-ium-1,2-diolate
• CAS No.: 955130-64-0
• Molecular Formula: C₂₈H₂₉ClN₄O₁₀
• Molecular Weight: 617.012

Synonyms:O₂-(acetoxymethyl) 1-{2-[2-[1-(4-chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetoxymethyloxycarbonyl]pyrrolidin-1-yl}diazen-1-ium-1,2-diolate

Chemical Property of O₂-(acetoxymethyl) 1-{2-[2-[1-(4-chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetoxymethyloxycarbonyl]pyrrolidin-1-yl}diazen-1-ium-1,2-diolate

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Technology Process of O₂-(acetoxymethyl) 1-{2-[2-[1-(4-chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetoxymethyloxycarbonyl]pyrrolidin-1-yl}diazen-1-ium-1,2-diolate

There total 2 articles about O₂-(acetoxymethyl) 1-{2-[2-[1-(4-chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetoxymethyloxycarbonyl]pyrrolidin-1-yl}diazen-1-ium-1,2-diolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

O2-(acetoxymethyl) 1-[2-(hydroxycarbonyl)pyrrolidin-1-yl]diazen-1-ium-1,2-diolate (955130-62-8) + chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate (154271-40-6) → C28H29ClN4O10 (955130-64-0)

Guidance literature:

O²-(acetoxymethyl) 1-[2-(hydroxycarbonyl)pyrrolidin-1-yl]diazen-1-ium-1,2-diolate; With triethylamine; In N,N-dimethyl-formamide; at 25 ℃; for 0.166667h;

chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate; In dimethyl sulfoxide; N,N-dimethyl-formamide; at 40 - 45 ℃; for 17h; Further stages.;

DOI:10.1021/jm701450q

Reference yield:

chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate (154271-40-6) + O2-(acetoxymethyl) 1-(2-(hydroxycarbonyl)pyrrolidin-1-yl)diazen-1-ium-1,2-diolate (955130-62-8) → O2-(acetoxymethyl) 1-{2-[2-[1-(4-chloro-benzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetoxymethyloxycarbonyl]pyrrolidin-1-yl}diazen-1-ium-1,2-diolate (955130-64-0)

Guidance literature:

O₂-(acetoxymethyl) 1-(2-(hydroxycarbonyl)pyrrolidin-1-yl)diazen-1-ium-1,2-diolate; With triethylamine; In dimethyl sulfoxide; at 25 ℃; for 0.0833333h;

chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate; In dimethyl sulfoxide; at 25 ℃; for 48h;

upstream raw materials:

O²-(acetoxymethyl) 1-[2-(hydroxycarbonyl)pyrrolidin-1-yl]diazen-1-ium-1,2-diolate

chloromethyl 2-[1-(4-chlorobenzoyl)-5-methoxy-2-methyl-1H-indol-3-yl]acetate

O₂-(acetoxymethyl) 1-(2-(hydroxycarbonyl)pyrrolidin-1-yl)diazen-1-ium-1,2-diolate

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