C₂₆H₃₁N₇O₄

Base Information

Chemical Name:C₂₆H₃₁N₇O₄
CAS No.:1392444-63-1
Molecular Formula:C₂₆H₃₁N₇O₄
Molecular Weight:505.577
Hs Code.:

C<sub>26</sub>H<sub>31</sub>N<sub>7</sub>O<sub>4</sub>

Synonyms:C₂₆H₃₁N₇O₄

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Chemical Property of C₂₆H₃₁N₇O₄

Chemical Property:

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Technology Process of C₂₆H₃₁N₇O₄

There total 8 articles about C₂₆H₃₁N₇O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 1314947-51-7
(R)-7-(3-tert-butoxycarbonylaminopiperidin-1-yl)-1-(2-cyanobenzyl)-3-methyl-5-methoxycarbonyl-2-oxo-2,3-dihydro-1H-imidazo[4,5-b]pyridine

: 1392444-63-1
C₂₆H₃₁N₇O₄

Guidance literature:: With ammonia; In 1-methyl-pyrrolidin-2-one; methanol; water; at 75 ℃; for 29h; Inert atmosphere;
DOI:10.1021/ml5001905

Reference yield:

: 4966-90-9
4-hydroxy-6-methyl-3-nitro-2(1H)-pyridinone

: 1392444-63-1
C₂₆H₃₁N₇O₄

Guidance literature:: Multi-step reaction with 9 steps

1: trichlorophosphate; N,N-dimethyl-aniline / 1.5 h / 95 °C / Inert atmosphere

2: sulfuric acid; chromium(VI) oxide / 2.5 h / 60 °C / Inert atmosphere

3: ethanol / 48 h / 20 °C / Inert atmosphere

4: ethanol; water / 48 h / 65 °C / Inert atmosphere

5: potassium hydroxide / tetrahydrofuran; water; diethyl ether / -20 °C / Inert atmosphere

6: palladium 10% on activated carbon; hydrogen / methanol / 3 h / Inert atmosphere

7: triethylamine / tetrahydrofuran / 0.5 h / -10 °C / Inert atmosphere

8: potassium carbonate / N,N-dimethyl-formamide / -10 °C / Inert atmosphere

9: ammonia / methanol; water; 1-methyl-pyrrolidin-2-one / 29 h / 75 °C / Inert atmosphere

With chromium(VI) oxide; sulfuric acid; palladium 10% on activated carbon; ammonia; hydrogen; potassium carbonate; N,N-dimethyl-aniline; triethylamine; potassium hydroxide; trichlorophosphate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ml5001905

Reference yield:

: 850544-26-2
2,4-dichloro-3-nitropyridine-6-carboxylic acid

: 1392444-63-1
C₂₆H₃₁N₇O₄

Guidance literature:: Multi-step reaction with 7 steps

1: ethanol / 48 h / 20 °C / Inert atmosphere

2: ethanol; water / 48 h / 65 °C / Inert atmosphere

3: potassium hydroxide / tetrahydrofuran; water; diethyl ether / -20 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / methanol / 3 h / Inert atmosphere

5: triethylamine / tetrahydrofuran / 0.5 h / -10 °C / Inert atmosphere

6: potassium carbonate / N,N-dimethyl-formamide / -10 °C / Inert atmosphere

7: ammonia / methanol; water; 1-methyl-pyrrolidin-2-one / 29 h / 75 °C / Inert atmosphere

With palladium 10% on activated carbon; ammonia; hydrogen; potassium carbonate; triethylamine; potassium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ml5001905