(S)-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-hydroxyethyl)-N-methylcarbamate

Base Information

Chemical Name:(S)-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-hydroxyethyl)-N-methylcarbamate
CAS No.:227618-90-8
Molecular Formula:C₃₁H₃₀ClNO₅
Molecular Weight:532.036
Hs Code.:

Synonyms:(S)-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-hydroxyethyl)-N-methylcarbamate

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Chemical Property of (S)-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-hydroxyethyl)-N-methylcarbamate

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Technology Process of (S)-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-hydroxyethyl)-N-methylcarbamate

There total 5 articles about (S)-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-hydroxyethyl)-N-methylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 227618-86-2
(2S-(2α(R*),3aα,4β,7β,7aα))-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-ethyl)-N-methylcarbamate

: 227618-90-8
(S)-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-hydroxyethyl)-N-methylcarbamate

Guidance literature:: With pyridinium p-toluenesulfonate; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1039/b008159k

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 227618-90-8
(S)-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-hydroxyethyl)-N-methylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / aq. NaOH / diethyl ether / Ambient temperature

2: 97 percent / LDA / tetrahydrofuran

3: 82 percent / HCl, MeOH / diethyl ether / Ambient temperature

With hydrogenchloride; methanol; sodium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1007/PL00010225

Reference yield:

: (2S-(2α,3aα,4β,7β,7aα))-3-chloro-α-((octahydro-7,8,8-trimethyl-4,7-methano-benzofuran-2-yl)oxy)-4,5-di(phenylmethoxy)-benzeneacetonitrile

: 227618-90-8
(S)-(phenylmethyl) N-(2-(3-chloro-4,5-di(phenylmethoxy)-phenyl)-2-hydroxyethyl)-N-methylcarbamate

Guidance literature:: Multi-step reaction with 4 steps

1: 38 percent / LiAlH₄ / diethyl ether

2: 97 percent / aq. NaOH / diethyl ether / Ambient temperature

3: 97 percent / LDA / tetrahydrofuran

4: 82 percent / HCl, MeOH / diethyl ether / Ambient temperature

With hydrogenchloride; methanol; sodium hydroxide; lithium aluminium tetrahydride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1007/PL00010225