N¹,N^1'-(ethane-1,2-diyl)bis(N³-(4-((E)-phenyldiazenyl)benzyl)propane-1,3-diamine)

Base Information

• Chemical Name: N¹,N^1'-(ethane-1,2-diyl)bis(N³-(4-((E)-phenyldiazenyl)benzyl)propane-1,3-diamine)
• CAS No.: 1610929-93-5
• Molecular Formula: C₃₄H₄₂N₈
• Molecular Weight: 562.761

Synonyms:N¹,N^1'-(ethane-1,2-diyl)bis(N³-(4-((E)-phenyldiazenyl)benzyl)propane-1,3-diamine)

Chemical Property of N¹,N^1'-(ethane-1,2-diyl)bis(N³-(4-((E)-phenyldiazenyl)benzyl)propane-1,3-diamine)

Chemical Property:

Purity/Quality:

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Technology Process of N¹,N^1'-(ethane-1,2-diyl)bis(N³-(4-((E)-phenyldiazenyl)benzyl)propane-1,3-diamine)

There total 9 articles about N¹,N^1'-(ethane-1,2-diyl)bis(N³-(4-((E)-phenyldiazenyl)benzyl)propane-1,3-diamine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

di-tert-butyl ethane-1,2-diylbis((3-((4-((E)-phenyldiazenyl)benzyl)amino)propyl)carbamate) (1610930-01-2) → N1,N1'-(ethane-1,2-diyl)bis(N3-(4-((E)-phenyldiazenyl)benzyl)propane-1,3-diamine) (1610929-93-5)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1002/chem.201304658

Reference yield:

2,2,2-Trifluoro-N-(3-{2-[3-(2,2,2-trifluoro-acetylamino)-propylamino]-ethylamino}-propyl)-acetamide (181181-34-0) → N1,N1'-(ethane-1,2-diyl)bis(N3-(4-((E)-phenyldiazenyl)benzyl)propane-1,3-diamine) (1610929-93-5)

Guidance literature:

Multi-step reaction with 5 steps

1: triethylamine / dichloromethane / 20 °C / Inert atmosphere

2: sodium hydroxide; water / ethanol / 20 °C / Inert atmosphere

3: ethanol / 24 h / Reflux; Molecular sieve; Inert atmosphere

4: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere

5: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; water; triethylamine; trifluoroacetic acid; sodium hydroxide; In methanol; ethanol; dichloromethane;

DOI:10.1002/chem.201304658

Reference yield:

(E)-(4-(phenyldiazenyl)phenyl)methanol (65926-74-1) → N1,N1'-(ethane-1,2-diyl)bis(N3-(4-((E)-phenyldiazenyl)benzyl)propane-1,3-diamine) (1610929-93-5)

Guidance literature:

Multi-step reaction with 4 steps

1: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

2: ethanol / 24 h / Reflux; Molecular sieve; Inert atmosphere

3: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With sodium tetrahydroborate; Dess-Martin periodane; trifluoroacetic acid; In methanol; ethanol; dichloromethane;

DOI:10.1002/chem.201304658

upstream raw materials:

N,N'-bis(3-aminopropyl)-1,2-diamine

2,2,2-Trifluoro-N-(3-{2-[3-(2,2,2-trifluoro-acetylamino)-propylamino]-ethylamino}-propyl)-acetamide

(E)-4-(phenyldiazenyl)benzoic acid

N,N'-(ethylenebis{[(tert-butoxycarbonyl)imino]propane-1,3-diyl})bis(trifluoroacetamide)

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