tris(cyclohexyl(methyl)amino)(1-cycloocten-5-ylamino)phosphonium chloride

Base Information

Chemical Name:tris(cyclohexyl(methyl)amino)(1-cycloocten-5-ylamino)phosphonium chloride
CAS No.:1380343-78-1
Molecular Formula:C₃₀H₅₈N₄P*Cl
Molecular Weight:541.244
Hs Code.:

Synonyms:tris(cyclohexyl(methyl)amino)(1-cycloocten-5-ylamino)phosphonium chloride

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Chemical Property of tris(cyclohexyl(methyl)amino)(1-cycloocten-5-ylamino)phosphonium chloride

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Technology Process of tris(cyclohexyl(methyl)amino)(1-cycloocten-5-ylamino)phosphonium chloride

There total 6 articles about tris(cyclohexyl(methyl)amino)(1-cycloocten-5-ylamino)phosphonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: tris(cyclohexyl(methyl)amino)(1-cycloocten-5-ylamino)phosphonium tetrafluoroborate

: 1380343-78-1
tris(cyclohexyl(methyl)amino)(1-cycloocten-5-ylamino)phosphonium chloride

Guidance literature:: With Amberlite-IRA 400(Cl) form; In methanol;
DOI:10.1021/ja307466s DOI:10.1021/ja307466s

Reference yield:

: tris(cyclohexylamino)(1-cycloocten-5-ylamino)phosphonium tetrafluoroborate

: 1380343-78-1
tris(cyclohexyl(methyl)amino)(1-cycloocten-5-ylamino)phosphonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / chlorobenzene / 8 h / 20 - 70 °C

2: Amberlite-IRA 400(Cl) form / methanol

With sodium hydroxide; In methanol; chlorobenzene;
DOI:10.1021/ja307466s DOI:10.1021/ja307466s

Reference yield:

: 5-azido-1-cyclooctene

: 1380343-78-1
tris(cyclohexyl(methyl)amino)(1-cycloocten-5-ylamino)phosphonium chloride

Guidance literature:: Multi-step reaction with 4 steps

1: phosphorus trichloride / toluene / 48 h / 70 °C

2: dichloromethane / 0 - 20 °C / Inert atmosphere

3: sodium hydroxide / chlorobenzene / 8 h / 20 - 70 °C

4: Amberlite-IRA 400(Cl) form / methanol

With sodium hydroxide; phosphorus trichloride; In methanol; dichloromethane; chlorobenzene; toluene;
DOI:10.1021/ja307466s DOI:10.1021/ja307466s