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tetrakis[cyclohexyl(methyl)amino]phosphonium methoxide

Base Information
  • Chemical Name:tetrakis[cyclohexyl(methyl)amino]phosphonium methoxide
  • CAS No.:1403962-13-9
  • Molecular Formula:CH3O*C28H56N4P
  • Molecular Weight:510.787
  • Hs Code.:
tetrakis[cyclohexyl(methyl)amino]phosphonium methoxide

Synonyms:tetrakis[cyclohexyl(methyl)amino]phosphonium methoxide

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Chemical Property of tetrakis[cyclohexyl(methyl)amino]phosphonium methoxide
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Technology Process of tetrakis[cyclohexyl(methyl)amino]phosphonium methoxide

There total 6 articles about tetrakis[cyclohexyl(methyl)amino]phosphonium methoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 6 steps
1: sodium azide / 48 h / 50 °C
2: phosphorus trichloride / toluene / 48 h / 70 °C
3: dichloromethane / 0 - 20 °C / Inert atmosphere
4: sodium hydroxide / chlorobenzene / 8 h / 20 - 70 °C
5: Amberlite-IRA 400(Cl) form / methanol
6: potassium hydroxide / water / 0.5 h
With sodium azide; potassium hydroxide; sodium hydroxide; phosphorus trichloride; In methanol; dichloromethane; water; chlorobenzene; toluene;
DOI:10.1021/ja307466s DOI:10.1021/ja307466s
Guidance literature:
Multi-step reaction with 3 steps
1: sodium hydroxide / chlorobenzene / 8 h / 20 - 70 °C
2: Amberlite-IRA 400(Cl) form / methanol
3: potassium hydroxide / water / 0.5 h
With potassium hydroxide; sodium hydroxide; In methanol; water; chlorobenzene;
DOI:10.1021/ja307466s DOI:10.1021/ja307466s
Guidance literature:
Multi-step reaction with 5 steps
1: phosphorus trichloride / toluene / 48 h / 70 °C
2: dichloromethane / 0 - 20 °C / Inert atmosphere
3: sodium hydroxide / chlorobenzene / 8 h / 20 - 70 °C
4: Amberlite-IRA 400(Cl) form / methanol
5: potassium hydroxide / water / 0.5 h
With potassium hydroxide; sodium hydroxide; phosphorus trichloride; In methanol; dichloromethane; water; chlorobenzene; toluene;
DOI:10.1021/ja307466s DOI:10.1021/ja307466s
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