4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]-N²-(4-chlorobenzoyl)benzhydrazide

Base Information

• Chemical Name: 4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]-N²-(4-chlorobenzoyl)benzhydrazide
• CAS No.: 895633-05-3
• Molecular Formula: C₂₄H₂₁ClN₆O₃
• Molecular Weight: 476.922

Synonyms:4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]-N²-(4-chlorobenzoyl)benzhydrazide

Chemical Property of 4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]-N²-(4-chlorobenzoyl)benzhydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]-N²-(4-chlorobenzoyl)benzhydrazide

There total 5 articles about 4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]-N²-(4-chlorobenzoyl)benzhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]benzhydrazide (895632-99-2) + 4-chloro-benzoyl chloride (122-01-0) → 4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]-N2-(4-chlorobenzoyl)benzhydrazide (895633-05-3)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃;

DOI:10.1246/bcsj.79.644

Reference yield:

ethyl 4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]benzoate (895632-95-8) → 4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]-N2-(4-chlorobenzoyl)benzhydrazide (895633-05-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 75 percent / hydrazine monohydrate / ethanol / Heating

2: 83 percent / pyridine / CH₂Cl₂ / 20 °C

With pyridine; hydrazine hydrate; In ethanol; dichloromethane;

DOI:10.1246/bcsj.79.644

Reference yield:

4-[4-(ethoxycarbonylphenylhydrazono)methyl-3-4-ethoxyphenyl]sydnone (895632-91-4) → 4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]-N2-(4-chlorobenzoyl)benzhydrazide (895633-05-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 50 percent / aq. HCl / ethyl acetate / 60 °C

2: 75 percent / hydrazine monohydrate / ethanol / Heating

3: 83 percent / pyridine / CH₂Cl₂ / 20 °C

With pyridine; hydrogenchloride; hydrazine hydrate; In ethanol; dichloromethane; ethyl acetate;

DOI:10.1246/bcsj.79.644

upstream raw materials:

4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]benzhydrazide

4-chloro-benzoyl chloride

ethyl 4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]benzoate

4-[4-(ethoxycarbonylphenylhydrazono)methyl-3-4-ethoxyphenyl]sydnone

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 895633-05-3 4-[4-(4-ethoxyphenylamino)-2H-1,2,3-triazol-2-yl]-N²-(4-chlorobenzoyl)benzhydrazide

Send

Send

Metric Ton KG G Pound L ML

Send

Send