2-(3-Phenyl-propylidene)-dithiomalonic acid di-S-ethyl ester

Base Information

• Chemical Name: 2-(3-Phenyl-propylidene)-dithiomalonic acid di-S-ethyl ester
• CAS No.: 137324-66-4
• Molecular Formula: C₁₆H₂₀O₂S₂
• Molecular Weight: 308.466
• Mol file: 137324-66-4.mol

Synonyms:2-(3-Phenyl-propylidene)-dithiomalonic acid di-S-ethyl ester

Chemical Property of 2-(3-Phenyl-propylidene)-dithiomalonic acid di-S-ethyl ester

Chemical Property:

Purity/Quality:

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Technology Process of 2-(3-Phenyl-propylidene)-dithiomalonic acid di-S-ethyl ester

There total 1 articles about 2-(3-Phenyl-propylidene)-dithiomalonic acid di-S-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-phenyl-propionaldehyde (104-53-0) + S,S'-diethyl dithiomalonate (16501-24-9) → 2-(3-Phenyl-propylidene)-dithiomalonic acid di-S-ethyl ester (137324-66-4) + 2-((E)-3-Phenyl-propenyl)-dithiomalonic acid di-S-ethyl ester (137324-67-5)

Guidance literature:

With 1,4-diaza-bicyclo[2.2.2]octane; sodium sulfate; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 48 h;

DOI:10.1080/00397919108019815

Reference yield: 20.0%

2-(3-Phenyl-propylidene)-dithiomalonic acid di-S-ethyl ester (137324-66-4) → 5-phenylpentan-1-ol (10521-91-2)

Guidance literature:

Ra-Ni; for 0.333333h;

DOI:10.1080/00397919108019815

upstream raw materials:

3-phenyl-propionaldehyde

S,S'-diethyl dithiomalonate

Downstream raw materials:

5-phenylpentan-1-ol