(S)-N-{5-(benzyloxy)-1-(tert-butyldiphenylsilyloxy)pentan-2-yl}-N-(3,4-dimethoxybenzyl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:(S)-N-{5-(benzyloxy)-1-(tert-butyldiphenylsilyloxy)pentan-2-yl}-N-(3,4-dimethoxybenzyl)-4-methylbenzenesulfonamide
CAS No.:1431116-48-1
Molecular Formula:C₄₄H₅₃NO₆SSi
Molecular Weight:752.059
Hs Code.:

Synonyms:(S)-N-{5-(benzyloxy)-1-(tert-butyldiphenylsilyloxy)pentan-2-yl}-N-(3,4-dimethoxybenzyl)-4-methylbenzenesulfonamide

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Chemical Property of (S)-N-{5-(benzyloxy)-1-(tert-butyldiphenylsilyloxy)pentan-2-yl}-N-(3,4-dimethoxybenzyl)-4-methylbenzenesulfonamide

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Technology Process of (S)-N-{5-(benzyloxy)-1-(tert-butyldiphenylsilyloxy)pentan-2-yl}-N-(3,4-dimethoxybenzyl)-4-methylbenzenesulfonamide

There total 6 articles about (S)-N-{5-(benzyloxy)-1-(tert-butyldiphenylsilyloxy)pentan-2-yl}-N-(3,4-dimethoxybenzyl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1431116-46-9
C₃₇H₄₇NO₆SSi

: 100-39-0
benzyl bromide

: 1431116-48-1
(S)-N-{5-(benzyloxy)-1-(tert-butyldiphenylsilyloxy)pentan-2-yl}-N-(3,4-dimethoxybenzyl)-4-methylbenzenesulfonamide

Guidance literature:: With sodium hydride; potassium iodide; In tetrahydrofuran; at 60 ℃; for 6h;
DOI:10.1016/j.tet.2013.03.012

Reference yield:

: C₂₃H₃₁NO₇S

: 1431116-48-1
(S)-N-{5-(benzyloxy)-1-(tert-butyldiphenylsilyloxy)pentan-2-yl}-N-(3,4-dimethoxybenzyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-imidazole / tetrahydrofuran / 24 h / 0 - 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C

3: potassium iodide; sodium hydride / tetrahydrofuran / 6 h / 60 °C

With 1H-imidazole; lithium aluminium tetrahydride; sodium hydride; potassium iodide; In tetrahydrofuran;
DOI:10.1016/j.tet.2013.03.012

Reference yield:

: C₃₉H₄₉NO₇SSi

: 1431116-48-1
(S)-N-{5-(benzyloxy)-1-(tert-butyldiphenylsilyloxy)pentan-2-yl}-N-(3,4-dimethoxybenzyl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 20 °C

2: potassium iodide; sodium hydride / tetrahydrofuran / 6 h / 60 °C

With lithium aluminium tetrahydride; sodium hydride; potassium iodide; In tetrahydrofuran;
DOI:10.1016/j.tet.2013.03.012