tert-Butyl {(phenylsulphonyl)[3-(trifluoromethyl)phenyl]methyl}-carbamate

Base Information

• Chemical Name: tert-Butyl {(phenylsulphonyl)[3-(trifluoromethyl)phenyl]methyl}-carbamate
• CAS No.: 1237534-74-5
• Molecular Formula: C₁₉H₂₀F₃NO₄S
• Molecular Weight: 415.433

Synonyms:tert-Butyl {(phenylsulphonyl)[3-(trifluoromethyl)phenyl]methyl}-carbamate

Chemical Property of tert-Butyl {(phenylsulphonyl)[3-(trifluoromethyl)phenyl]methyl}-carbamate

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Technology Process of tert-Butyl {(phenylsulphonyl)[3-(trifluoromethyl)phenyl]methyl}-carbamate

There total 1 articles about tert-Butyl {(phenylsulphonyl)[3-(trifluoromethyl)phenyl]methyl}-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

tert-butyl carbazate (4248-19-5) + 3-Trifluoromethylbenzaldehyde (454-89-7) + sodium benzenesulfonate (873-55-2) → tert-Butyl {(phenylsulphonyl)[3-(trifluoromethyl)phenyl]methyl}-carbamate (1237534-74-5)

Guidance literature:

With formic acid; In methanol; water; at 20 ℃; for 30h;

Reference yield: 100.0%

tert-Butyl {(phenylsulphonyl)[3-(trifluoromethyl)phenyl]methyl}-carbamate (1237534-74-5) → tert-Butyl {(E)-[3-(trifluoromethyl)phenyl]methylidene}carbamate (1245622-09-6)

Guidance literature:

With potassium carbonate; In tetrahydrofuran; for 16h; Inert atmosphere; Reflux;

Reference yield: 88.0%

Sesamol (533-31-3) + tert-Butyl {(phenylsulphonyl)[3-(trifluoromethyl)phenyl]methyl}-carbamate (1237534-74-5) → tert-butyl [(6-hydroxybenzo[d][1,3]dioxol-5-yl)(3-(trifluoromethyl)phenyl)methyl]carbamate (1237534-93-8)

Guidance literature:

With cetyltrimethylammonim bromide; sodium carbonate; In water; at 30 ℃; for 10h;

DOI:10.1055/s-0029-1219802

upstream raw materials:

tert-butyl carbazate

3-Trifluoromethylbenzaldehyde

sodium benzenesulfonate

Downstream raw materials:

tert-butyl [(6-hydroxybenzo[d][1,3]dioxol-5-yl)(3-(trifluoromethyl)phenyl)methyl]carbamate

tert-Butyl {(E)-[3-(trifluoromethyl)phenyl]methylidene}carbamate

tert-Butyl {[3-(trifluoromethyl)phenyl](1-trityl-1H-imidazol-4-yl)methyl}carbamate

tert-Butyl {1,3-oxazol-2-yl[3-(trifluoromethyl)phenyl]methyl}carbamate

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