tert-Butyl {[3-(trifluoromethyl)phenyl](1-trityl-1H-imidazol-4-yl)methyl}carbamate

Base Information

Chemical Name:tert-Butyl {[3-(trifluoromethyl)phenyl](1-trityl-1H-imidazol-4-yl)methyl}carbamate
CAS No.:1268635-99-9
Molecular Formula:C₃₅H₃₂F₃N₃O₂
Molecular Weight:583.653
Hs Code.:

Synonyms:tert-Butyl {[3-(trifluoromethyl)phenyl](1-trityl-1H-imidazol-4-yl)methyl}carbamate

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Chemical Property of tert-Butyl {[3-(trifluoromethyl)phenyl](1-trityl-1H-imidazol-4-yl)methyl}carbamate

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Technology Process of tert-Butyl {[3-(trifluoromethyl)phenyl](1-trityl-1H-imidazol-4-yl)methyl}carbamate

There total 4 articles about tert-Butyl {[3-(trifluoromethyl)phenyl](1-trityl-1H-imidazol-4-yl)methyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 1245622-09-6
tert-Butyl {(E)-[3-(trifluoromethyl)phenyl]methylidene}carbamate

: 96797-15-8
N-trityl-4⁽⁵⁾-iodoimidazole

: 1268635-99-9
tert-Butyl {[3-(trifluoromethyl)phenyl](1-trityl-1H-imidazol-4-yl)methyl}carbamate

Guidance literature:: N-trityl-4⁽⁵⁾-iodoimidazole; With ethylmagnesium bromide; In diethyl ether; dichloromethane; at 20 ℃; for 0.5h;

tert-Butyl {(E)-[3-(trifluoromethyl)phenyl]methylidene}carbamate; In diethyl ether; dichloromethane; at 20 ℃;

Reference yield:

: 4248-19-5
tert-butyl carbazate

: 1268635-99-9
tert-Butyl {[3-(trifluoromethyl)phenyl](1-trityl-1H-imidazol-4-yl)methyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: formic acid / water; methanol / 30 h / 20 °C

2.1: potassium carbonate / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

3.1: ethylmagnesium bromide / dichloromethane; diethyl ether / 0.5 h / 20 °C

3.2: 20 °C

With formic acid; ethylmagnesium bromide; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water;

Reference yield:

: 1237534-74-5
tert-Butyl {(phenylsulphonyl)[3-(trifluoromethyl)phenyl]methyl}-carbamate

: 1268635-99-9
tert-Butyl {[3-(trifluoromethyl)phenyl](1-trityl-1H-imidazol-4-yl)methyl}carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

2.1: ethylmagnesium bromide / dichloromethane; diethyl ether / 0.5 h / 20 °C

2.2: 20 °C

With ethylmagnesium bromide; potassium carbonate; In tetrahydrofuran; diethyl ether; dichloromethane;