Technology Process of C29H36O4S
There total 15 articles about C29H36O4S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium carbonate;
In
N,N-dimethyl-formamide;
at 55 ℃;
for 5h;
DOI:10.1021/ja044123l
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 96 percent / Et3N / CH2Cl2 / 0.75 h / -78 °C
2: 76 percent / Li2CO3 / dimethylformamide / 5 h / 55 °C
With
lithium carbonate; triethylamine;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja044123l
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 94 percent / P(OMe)3; O2; t-BuOK / tetrahydrofuran; 2-methyl-propan-2-ol / 0.75 h / -40 °C
2: 73 percent / VO(acac)2; t-BuOOH / benzene; decane / 10 h / 20 °C
3: 72 percent / Et3N / CH2Cl2 / 1 h / -10 - -5 °C
4: NaBH4 / methanol / 5 h / 20 °C
5: 39 mg / PPTS / CH2Cl2 / 0.5 h / Heating
6: 90 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH2Cl2 / 18 h / 20 °C
7: 96 percent / Et3N / CH2Cl2 / 0.75 h / -78 °C
8: 76 percent / Li2CO3 / dimethylformamide / 5 h / 55 °C
With
tert.-butylhydroperoxide; sodium tetrahydroborate; bis(acetylacetonate)oxovanadium; potassium tert-butylate; oxygen; pyridinium p-toluenesulfonate; lithium carbonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; phosphorous acid trimethyl ester;
In
tetrahydrofuran; methanol; decane; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol; benzene;
DOI:10.1021/ja044123l
