1-cyclohex-3-enylmethyl acetate; methane

Base Information

• Chemical Name: 1-cyclohex-3-enylmethyl acetate; methane
• CAS No.: 74454-29-8
• Molecular Formula: C10H18O2
• Molecular Weight: 168.236
• Mol file: 74454-29-8.mol

Synonyms:EINECS 277-879-4;1-phenylethyl acetate;

Chemical Property of 1-cyclohex-3-enylmethyl acetate; methane

Chemical Property:

• Boiling Point: 195.3oC at 760 mmHg
• Flash Point: 80.8oC
• PSA: 26.30000
• LogP: 2.29430

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-cyclohex-3-enylmethyl acetate; methane

There total 4 articles about 1-cyclohex-3-enylmethyl acetate; methane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Cyclohexene-1-carboxaldehyde (100-50-5,61746-36-9) → 1-phenylethyl acetate (74454-29-8)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium chips, methyl iodide / diethyl ether / 0.25 h / Heating

2: pyridine / 0.5 h / Heating

With pyridine; magnesium; methyl iodide; In diethyl ether;

Reference yield:

4-(1-hydroxyethyl)-1-cyclohexene (17264-01-6) + acetic anhydride (108-24-7) → 1-phenylethyl acetate (74454-29-8)

Guidance literature:

With sulfuric acid;

Reference yield:

4-(1-hydroxyethyl)-1-cyclohexene (17264-01-6) + acetyl chloride (75-36-5) → 1-phenylethyl acetate (74454-29-8)

Guidance literature:

With pyridine; for 0.5h; Heating;

upstream raw materials:

4-(1-hydroxyethyl)-1-cyclohexene

acetic anhydride

acetyl chloride

4-ethenylcyclohexene

Downstream raw materials:

4-ethenylcyclohexene

Refernces

• 1、 Guiotto,Manzini,Pastorini,Rodighiero. "Synthesis and attractiveness for Ceratitis capitata Wied. Males of Δ3cyclohexenylalkylcarbinol acetates. IV (1)". . p. 441 - 446. Retrieved 2007/10/02.