Methyl 2,3-di-O-benzoyl-4,6-dideoxy-4-(2',4'-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside

Base Information

Chemical Name:Methyl 2,3-di-O-benzoyl-4,6-dideoxy-4-(2',4'-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside
CAS No.:163072-30-8
Molecular Formula:C₃₉H₃₇NO₁₁
Molecular Weight:695.723
Hs Code.:

Synonyms:Methyl 2,3-di-O-benzoyl-4,6-dideoxy-4-(2',4'-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside

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Chemical Property of Methyl 2,3-di-O-benzoyl-4,6-dideoxy-4-(2',4'-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside

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Technology Process of Methyl 2,3-di-O-benzoyl-4,6-dideoxy-4-(2',4'-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside

There total 1 articles about Methyl 2,3-di-O-benzoyl-4,6-dideoxy-4-(2',4'-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 98-88-4
benzoyl chloride

: 116786-66-4
methyl 4,6-dideoxy-4-(3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside

: 163072-30-8
Methyl 2,3-di-O-benzoyl-4,6-dideoxy-4-(2',4'-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside

Guidance literature:: With pyridine; Ambient temperature;

Reference yield: 81.5%

: 163072-30-8
Methyl 2,3-di-O-benzoyl-4,6-dideoxy-4-(2',4'-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside

: 163072-31-9
2,3-Di-O-benzoyl-4,6-dideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranosyl chloride

Guidance literature:: With Dichloromethyl methyl ether; zinc(II) chloride; In chloroform; at 50 ℃; for 2h;

Reference yield:

: 163072-30-8
Methyl 2,3-di-O-benzoyl-4,6-dideoxy-4-(2',4'-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside

: 163072-32-0
Methyl 2-O-<2,3-di-O-benzoyl-4,6-dideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranosyl>-4,6-dideoxy-4-(2,4-di-O-benzoyl-3-deoxy-L-glycero-tetronamido)-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 81.5 percent / ZnCl₂, dichloromethyl methyl ether / CHCl₃ / 2 h / 50 °C

2: 81 percent / 2,4,6-trimethylpyridine, AgOTf / CH₂Cl₂ / 1 h / 0 °C

3: 100 percent / H₂ / 5percent Pd/C / acetone; ethanol

With 2,4,6-trimethyl-pyridine; Dichloromethyl methyl ether; hydrogen; silver trifluoromethanesulfonate; zinc(II) chloride; palladium on activated charcoal; In ethanol; dichloromethane; chloroform; acetone;