4-(toluene-4-sulfonyloxymethyl)-cyclohexane carboxylic acid methyl ester

Base Information

Chemical Name:4-(toluene-4-sulfonyloxymethyl)-cyclohexane carboxylic acid methyl ester
CAS No.:1003013-11-3
Molecular Formula:C₁₆H₂₂O₅S
Molecular Weight:326.414
Hs Code.:

Synonyms:4-(toluene-4-sulfonyloxymethyl)-cyclohexane carboxylic acid methyl ester

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Chemical Property of 4-(toluene-4-sulfonyloxymethyl)-cyclohexane carboxylic acid methyl ester

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Technology Process of 4-(toluene-4-sulfonyloxymethyl)-cyclohexane carboxylic acid methyl ester

There total 1 articles about 4-(toluene-4-sulfonyloxymethyl)-cyclohexane carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 13380-85-3
4-hydroxymethylcyclohexanecarboxylic acid methyl ester

: 98-59-9
p-toluenesulfonyl chloride

: 1003013-11-3
4-(toluene-4-sulfonyloxymethyl)-cyclohexane carboxylic acid methyl ester

Guidance literature:: With pyridine; In dichloromethane; at 25 ℃; for 16h;

Reference yield: 37.0%

: 1003013-11-3
4-(toluene-4-sulfonyloxymethyl)-cyclohexane carboxylic acid methyl ester

: 1003013-12-4
4-(3-nitro-pyrazol-1-ylmethyl)-cyclohexanecarboxylic acid methyl ester

Guidance literature:: 3-nitro-1H-pyrazole; With sodium hydride; In N,N-dimethyl-formamide; for 0.166667h;

4-(toluene-4-sulfonyloxymethyl)-cyclohexane carboxylic acid methyl ester; In N,N-dimethyl-formamide; at 80 ℃; for 6h;

Reference yield:

: 1003013-11-3
4-(toluene-4-sulfonyloxymethyl)-cyclohexane carboxylic acid methyl ester

: 4-{3-[2-(R)-(3-chloro-4-methanesulfonyl-phenyl)-3-cyclopentyl-propionylamino]-pyrazol-1-ylmethyl}-cyclohexanecarboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h

1.2: 6 h / 80 °C

2.1: hydrazine / nickel / methanol; water; ethyl acetate / 0.5 h

3.1: oxalyl dichloride / dichloromethane / 0.25 h / 25 °C

3.2: 0.25 h / 0 °C

3.3: 0.42 h / 0 - 25 °C

With oxalyl dichloride; sodium hydride; hydrazine; nickel; In methanol; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;