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Technology Process of C37H37BF2N4

C37H37BF2N4

Base Information
  • Chemical Name:C37H37BF2N4
  • CAS No.:1239971-44-8
  • Molecular Formula:C37H37BF2N4
  • Molecular Weight:586.535
  • Hs Code.:
C<sub>37</sub>H<sub>37</sub>BF<sub>2</sub>N<sub>4</sub>

Synonyms:C37H37BF2N4

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Chemical Property of C37H37BF2N4
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Technology Process of C37H37BF2N4

There total 3 articles about C37H37BF2N4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

C<sub>41</sub>H<sub>41</sub>BF<sub>2</sub>N<sub>4</sub>O<sub>2</sub>
1239971-42-6

C41H41BF2N4O2

C<sub>37</sub>H<sub>37</sub>BF<sub>2</sub>N<sub>4</sub>
1239971-44-8

C37H37BF2N4

Guidance literature:
C41H41BF2N4O2; With hydrogenchloride; In methanol; water; at 100 ℃; for 6h;
With boron trifluoride diethyl etherate; triethylamine; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2010.03.013

Reference yield:

benzaldehyde
100-52-7

benzaldehyde

C<sub>37</sub>H<sub>37</sub>BF<sub>2</sub>N<sub>4</sub>
1239971-44-8

C37H37BF2N4

Guidance literature:
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid
1.3: 20 °C / Inert atmosphere
2.1: piperidine; acetic acid / toluene / Dean-Stark; Reflux
3.1: hydrogenchloride / ethanol; water
With piperidine; hydrogenchloride; acetic acid; trifluoroacetic acid; In ethanol; water; toluene;
DOI:10.1002/chem.202003574

Reference yield:

2,4-dimethyl-3-ethyl-pyrrole
517-22-6

2,4-dimethyl-3-ethyl-pyrrole

C<sub>37</sub>H<sub>37</sub>BF<sub>2</sub>N<sub>4</sub>
1239971-44-8

C37H37BF2N4

Guidance literature:
Multi-step reaction with 3 steps
1.1: trifluoroacetic acid
1.3: 20 °C / Inert atmosphere
2.1: piperidine; acetic acid / toluene / Dean-Stark; Reflux
3.1: hydrogenchloride / ethanol; water
With piperidine; hydrogenchloride; acetic acid; trifluoroacetic acid; In ethanol; water; toluene;
DOI:10.1002/chem.202003574
upstream raw materials:

C41H41BF2N4O2

benzaldehyde

2,4-dimethyl-3-ethyl-pyrrole

Downstream raw materials:

C51H49BF2N4O2

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