3-(2-(4-[(2-aminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzamidine

Base Information

Chemical Name:3-(2-(4-[(2-aminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzamidine
CAS No.:330939-58-7
Molecular Formula:C₂₆H₂₁N₅O₆S
Molecular Weight:531.549
Hs Code.:

Synonyms:3-(2-(4-[(2-aminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzamidine

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Chemical Property of 3-(2-(4-[(2-aminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzamidine

Chemical Property:

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Technology Process of 3-(2-(4-[(2-aminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzamidine

There total 8 articles about 3-(2-(4-[(2-aminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 330942-81-9
3-(2-(4-[(2-t-butylaminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzonitrile

: 330939-58-7
3-(2-(4-[(2-aminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzamidine

Guidance literature:: 3-(2-(4-[(2-t-butylaminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzonitrile; With hydrogenchloride; In methanol; at 0 - 20 ℃;

With ammonium acetate; In methanol; for 2h; Reflux;

Reference yield:

: 873-62-1
m-cyanophenol

: 330939-58-7
3-(2-(4-[(2-aminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzamidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: K₂CO₃ / dimethylformamide

2.1: AlMe₃ / CH₂Cl₂

3.1: HCl(g) / methanol

3.2: NH₄OAc / methanol

With hydrogenchloride; trimethylaluminum; potassium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00234-2

Reference yield:

: 7304-32-7
2-fluoro-5-nitrobenzoic acid

: 330939-58-7
3-(2-(4-[(2-aminosulfonyl)phenyl]phenyl)aminocarbonyl-4-nitrophenoxy)benzamidine

Guidance literature:: Multi-step reaction with 4 steps

1.1: methanol

2.1: K₂CO₃ / dimethylformamide

3.1: AlMe₃ / CH₂Cl₂

4.1: HCl(g) / methanol

4.2: NH₄OAc / methanol

With hydrogenchloride; trimethylaluminum; potassium carbonate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0960-894X(02)00234-2