1-(4-methylimidazol-5-yl-carbonyl)-4-(4-methylphenyl)thiosemicarbazide

Base Information

• Chemical Name: 1-(4-methylimidazol-5-yl-carbonyl)-4-(4-methylphenyl)thiosemicarbazide
• CAS No.: 1260230-17-8
• Molecular Formula: C₁₃H₁₅N₅OS
• Molecular Weight: 289.361
• Mol file: 1260230-17-8.mol

Synonyms:1-(4-methylimidazol-5-yl-carbonyl)-4-(4-methylphenyl)thiosemicarbazide

Chemical Property of 1-(4-methylimidazol-5-yl-carbonyl)-4-(4-methylphenyl)thiosemicarbazide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 1-(4-methylimidazol-5-yl-carbonyl)-4-(4-methylphenyl)thiosemicarbazide

There total 1 articles about 1-(4-methylimidazol-5-yl-carbonyl)-4-(4-methylphenyl)thiosemicarbazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

4-methylimidazol-5-yl-carboxylic acid hydrazide (71704-67-1) + 1-isothiocyanato-4-methylbenzene (622-59-3) → 1-(4-methylimidazol-5-yl-carbonyl)-4-(4-methylphenyl)thiosemicarbazide (1260230-17-8)

Guidance literature:

In diethyl ether; at 80 ℃; for 12h;

DOI:10.1002/hc.20643

Reference yield: 40.0%

1-(4-methylimidazol-5-yl-carbonyl)-4-(4-methylphenyl)thiosemicarbazide (1260230-17-8) → 5-(4-methylimidazol-5-yl)-4-(4-methylphenyl)-s-triazole-3-thione (1260230-23-6)

Guidance literature:

1-(4-methylimidazol-5-yl-carbonyl)-4-(4-methylphenyl)thiosemicarbazide; With sodium hydroxide; In water; for 2h; Reflux;

With hydrogenchloride; In water;

DOI:10.1002/hc.20643

upstream raw materials:

4-methylimidazol-5-yl-carboxylic acid hydrazide

1-isothiocyanato-4-methylbenzene

Downstream raw materials:

5-(4-methylimidazol-5-yl)-4-(4-methylphenyl)-s-triazole-3-thione