benzyl 2,3,5,6-tetra-O-tert-butyldimethylsilyl-1-thio-β-D-galactofuranoside

Base Information

• Chemical Name: benzyl 2,3,5,6-tetra-O-tert-butyldimethylsilyl-1-thio-β-D-galactofuranoside
• CAS No.: 1415315-81-9
• Molecular Formula: C₃₇H₇₄O₅SSi₄
• Molecular Weight: 743.4

Synonyms:benzyl 2,3,5,6-tetra-O-tert-butyldimethylsilyl-1-thio-β-D-galactofuranoside

Chemical Property of benzyl 2,3,5,6-tetra-O-tert-butyldimethylsilyl-1-thio-β-D-galactofuranoside

Chemical Property:

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Technology Process of benzyl 2,3,5,6-tetra-O-tert-butyldimethylsilyl-1-thio-β-D-galactofuranoside

There total 1 articles about benzyl 2,3,5,6-tetra-O-tert-butyldimethylsilyl-1-thio-β-D-galactofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3,5,6-tetra-O-tert-butyldimethylsilyl-1-thio-α,β-D-galactofuranose + benzyl bromide (100-39-0) → benzyl 2,3,5,6-tetra-O-tert-butyldimethylsilyl-1-thio-β-D-galactofuranoside (1415315-81-9) + benzyl 2,3,5,6-tetra-O-tert-butyldimethylsilyl-1-thio-α-D-galactofuranoside (1415315-82-0)

Guidance literature:

With tetra(n-butyl)ammonium hydrogensulfate; sodium hydrogencarbonate; In ethyl acetate; at 20 ℃; for 48h; pH=8.5; Overall yield = 80 %; Overall yield = 0.041 g;

DOI:10.1016/j.carres.2012.08.021

upstream raw materials:

benzyl bromide

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