2-Phenyl-3b,4,5,6,7,8-hexahydro-1H-3,3a-diaza-cyclopenta[1,3]cyclopropa[1,2]cycloheptene

Base Information

• Chemical Name: 2-Phenyl-3b,4,5,6,7,8-hexahydro-1H-3,3a-diaza-cyclopenta[1,3]cyclopropa[1,2]cycloheptene
• CAS No.: 73594-37-3
• Molecular Formula: C₁₅H₁₈N₂
• Molecular Weight: 226.321

Synonyms:2-Phenyl-3b,4,5,6,7,8-hexahydro-1H-3,3a-diaza-cyclopenta[1,3]cyclopropa[1,2]cycloheptene

Chemical Property of 2-Phenyl-3b,4,5,6,7,8-hexahydro-1H-3,3a-diaza-cyclopenta[1,3]cyclopropa[1,2]cycloheptene

Chemical Property:

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Technology Process of 2-Phenyl-3b,4,5,6,7,8-hexahydro-1H-3,3a-diaza-cyclopenta[1,3]cyclopropa[1,2]cycloheptene

There total 8 articles about 2-Phenyl-3b,4,5,6,7,8-hexahydro-1H-3,3a-diaza-cyclopenta[1,3]cyclopropa[1,2]cycloheptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

α-(cyclohepten-1-yl)acetophenone N-tosylhydrazone (73594-34-0) → 2-Phenyl-3b,4,5,6,7,8-hexahydro-1H-3,3a-diaza-cyclopenta[1,3]cyclopropa[1,2]cycloheptene (73594-37-3)

Guidance literature:

With sodium hydride; In tetrachloromethane; Heating;

DOI:10.1021/ja00523a051

Reference yield: 58.0%

α-(cyclohepten-1-yl)acetophenone N-tosylhydrazone (73594-34-0) + dimethylfumarate (624-49-7) → 2-Phenyl-3b,4,5,6,7,8-hexahydro-1H-3,3a-diaza-cyclopenta[1,3]cyclopropa[1,2]cycloheptene (73594-37-3) + (4S,5R)-5-Cyclohept-1-enylmethyl-5-phenyl-4,5-dihydro-1H-pyrazole-3,4-dicarboxylic acid dimethyl ester (100188-64-5) + (4R,5R)-5-Cyclohept-1-enylmethyl-5-phenyl-4,5-dihydro-1H-pyrazole-3,4-dicarboxylic acid dimethyl ester (100188-65-6)

Guidance literature:

With sodium hydride; In tetrachloromethane; Product distribution; Mechanism; Heating; other tosylhydrazones;

DOI:10.1021/ja00523a051

Reference yield: 20.0%

sodium salt of α-(cyclohepten-1-yl)-acetophenone N-tosylhydrazone (100188-63-4) + dimethylfumarate (624-49-7) → 2-Phenyl-3b,4,5,6,7,8-hexahydro-1H-3,3a-diaza-cyclopenta[1,3]cyclopropa[1,2]cycloheptene (73594-37-3) + sodium 4-methylbenzenesulfinate (824-79-3) + (4S,5R)-5-Cyclohept-1-enylmethyl-5-phenyl-4,5-dihydro-1H-pyrazole-3,4-dicarboxylic acid dimethyl ester (100188-64-5) + (4R,5R)-5-Cyclohept-1-enylmethyl-5-phenyl-4,5-dihydro-1H-pyrazole-3,4-dicarboxylic acid dimethyl ester (100188-65-6)

Guidance literature:

In tetrachloromethane; for 0.5h; Heating;

DOI:10.1021/ja00267a036

upstream raw materials:

α-(cyclohepten-1-yl)acetophenone N-tosylhydrazone

1-(2-Diazo-2-phenyl-ethyl)-cycloheptene

sodium salt of α-(cyclohepten-1-yl)-acetophenone N-tosylhydrazone

dimethylfumarate

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