(3S,4R,5R,6R)-6-(tert-butyldimethylsilyloxy)-4-methoxy-8-(4-methoxybenzyloxy)-3,5-dimethyloctanenitrile

Base Information

Chemical Name:(3S,4R,5R,6R)-6-(tert-butyldimethylsilyloxy)-4-methoxy-8-(4-methoxybenzyloxy)-3,5-dimethyloctanenitrile
CAS No.:1217869-97-0
Molecular Formula:C₂₅H₄₃NO₄Si
Molecular Weight:449.706
Hs Code.:

Synonyms:(3S,4R,5R,6R)-6-(tert-butyldimethylsilyloxy)-4-methoxy-8-(4-methoxybenzyloxy)-3,5-dimethyloctanenitrile

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Chemical Property of (3S,4R,5R,6R)-6-(tert-butyldimethylsilyloxy)-4-methoxy-8-(4-methoxybenzyloxy)-3,5-dimethyloctanenitrile

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Technology Process of (3S,4R,5R,6R)-6-(tert-butyldimethylsilyloxy)-4-methoxy-8-(4-methoxybenzyloxy)-3,5-dimethyloctanenitrile

There total 1 articles about (3S,4R,5R,6R)-6-(tert-butyldimethylsilyloxy)-4-methoxy-8-(4-methoxybenzyloxy)-3,5-dimethyloctanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 773837-37-9
sodium cyanide

: 500220-29-1
(2S,3R,4S,5R)-5-(tert-butyldimethylsilanyloxy)-3-methoxy-7-(4-methoxybenzyloxy)-2,4-dimethylheptyl 4-methylbenzenesulfonate

: 1217869-97-0
(3S,4R,5R,6R)-6-(tert-butyldimethylsilyloxy)-4-methoxy-8-(4-methoxybenzyloxy)-3,5-dimethyloctanenitrile

Guidance literature:: In dimethyl sulfoxide; at 80 ℃; for 2h;
DOI:10.1055/s-0029-1217099

Reference yield: 100.0%

: 1217869-97-0
(3S,4R,5R,6R)-6-(tert-butyldimethylsilyloxy)-4-methoxy-8-(4-methoxybenzyloxy)-3,5-dimethyloctanenitrile

: 1217869-89-0
(3S,4R,5R,6R)-6-(tert-butyldimethylsilyloxy)-4-methoxy-8-(4-methoxybenzyloxy)-3,5-dimethyloctanal

Guidance literature:: (3S,4R,5R,6R)-6-(tert-butyldimethylsilyloxy)-4-methoxy-8-(4-methoxybenzyloxy)-3,5-dimethyloctanenitrile; With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃;

With water; rochelle salt; In hexane; dichloromethane;
DOI:10.1055/s-0029-1217099