C₃₃H₃₄BN₃O₉

Base Information

Chemical Name:C₃₃H₃₄BN₃O₉
CAS No.:1425051-95-1
Molecular Formula:C₃₃H₃₄BN₃O₉
Molecular Weight:627.459
Hs Code.:

C<sub>33</sub>H<sub>34</sub>BN<sub>3</sub>O<sub>9</sub>

Synonyms:C₃₃H₃₄BN₃O₉

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Chemical Property of C₃₃H₃₄BN₃O₉

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Technology Process of C₃₃H₃₄BN₃O₉

There total 10 articles about C₃₃H₃₄BN₃O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1425051-93-9
C₂₆H₃₀BNO₆

: 100-28-7
4-Nitrophenyl isocyanate

: 1425051-95-1
C₃₃H₃₄BN₃O₉

Guidance literature:: With triethylamine; In tetrahydrofuran; at 23 ℃; for 1.5h; Inert atmosphere;
DOI:10.1021/jo400105m

Reference yield:

: 1404094-91-2
(2‐methoxy‐4‐(4,4,5,5‐tetramethyl‐1,3,2‐dioxaborolan‐2‐yl)phenyl)methanol

: 1425051-95-1
C₃₃H₃₄BN₃O₉

Guidance literature:: Multi-step reaction with 3 steps

1.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere

1.2: 3 h / 85 °C / Inert atmosphere

2.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere

2.2: 24 h / 23 °C / Inert atmosphere

3.1: triethylamine / tetrahydrofuran / 1.5 h / 23 °C / Inert atmosphere

With diphenylphosphoranyl azide; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; water; benzene; 1.1: |Curtius Rearrangement / 1.2: |Curtius Rearrangement;
DOI:10.1021/jo400105m

Reference yield:

: 73183-34-3
bis(pinacol)diborane

: 1425051-95-1
C₃₃H₃₄BN₃O₉

Guidance literature:: Multi-step reaction with 4 steps

1.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; 1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate / 1,4-dioxane / 48 h / 80 °C / Inert atmosphere

2.1: diphenylphosphoranyl azide; triethylamine / benzene / 1 h / 85 °C / Inert atmosphere

2.2: 3 h / 85 °C / Inert atmosphere

3.1: toluene-4-sulfonic acid / tetrahydrofuran; water / 14 h / 23 °C / Inert atmosphere

3.2: 24 h / 23 °C / Inert atmosphere

4.1: triethylamine / tetrahydrofuran / 1.5 h / 23 °C / Inert atmosphere

With 1,1'-bis-(diphenylphosphino)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; diphenylphosphoranyl azide; potassium acetate; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; 1,4-dioxane; water; benzene; 1.1: |Miyaura Borylation Reaction / 2.1: |Curtius Rearrangement / 2.2: |Curtius Rearrangement;
DOI:10.1021/jo400105m