6,7,8,14-tetrahydro-7α-(α-hydroxy-α-methylbenzyl)-6,14-endo-ethanothebaine

Base Information

Chemical Name:6,7,8,14-tetrahydro-7α-(α-hydroxy-α-methylbenzyl)-6,14-endo-ethanothebaine
CAS No.:16196-72-8
Molecular Formula:C₂₉H₃₅NO₄
Molecular Weight:461.601
Hs Code.:

Synonyms:6,7,8,14-tetrahydro-7α-(α-hydroxy-α-methylbenzyl)-6,14-endo-ethanothebaine

Suppliers and Price of 6,7,8,14-tetrahydro-7α-(α-hydroxy-α-methylbenzyl)-6,14-endo-ethanothebaine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6,7,8,14-tetrahydro-7α-(α-hydroxy-α-methylbenzyl)-6,14-endo-ethanothebaine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6,7,8,14-tetrahydro-7α-(α-hydroxy-α-methylbenzyl)-6,14-endo-ethanothebaine

There total 4 articles about 6,7,8,14-tetrahydro-7α-(α-hydroxy-α-methylbenzyl)-6,14-endo-ethanothebaine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 917-64-6
methyl magnesium iodide

: 182325-11-7
Dihydronepenthone

: 16196-72-8
6,7,8,14-tetrahydro-7α-(α-hydroxy-α-methylbenzyl)-6,14-endo-ethanothebaine

Guidance literature:: In tetrahydrofuran; toluene; for 1h; Heating;
DOI:10.1016/S0968-0896(96)00257-X

Reference yield:

: 16180-37-3
(5R,6R,7R,9R,13S,14R,20S)-4,5-Epoxy-3,6-dimethoxy-α,17-dimethyl-α-phenyl-6,14-ethenomorphinan-7-methanol

: 16196-72-8
6,7,8,14-tetrahydro-7α-(α-hydroxy-α-methylbenzyl)-6,14-endo-ethanothebaine

Guidance literature:: With hydrogen; nickel; In ethanol;
DOI:10.1021/ja00989a031

Reference yield:

: phenylmagnesium bromide

: 16196-72-8
6,7,8,14-tetrahydro-7α-(α-hydroxy-α-methylbenzyl)-6,14-endo-ethanothebaine

Guidance literature:: Multi-step reaction with 2 steps

2: H₂ / Raney-Ni / ethanol

With hydrogen; nickel; In ethanol;
DOI:10.1021/ja00989a031