C₃₄H₄₆O₅

Base Information

Chemical Name:C₃₄H₄₆O₅
CAS No.:1186505-20-3
Molecular Formula:C₃₄H₄₆O₅
Molecular Weight:534.736
Hs Code.:

C<sub>34</sub>H<sub>46</sub>O<sub>5</sub>

Synonyms:C₃₄H₄₆O₅

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Chemical Property of C₃₄H₄₆O₅

Chemical Property:

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Technology Process of C₃₄H₄₆O₅

There total 11 articles about C₃₄H₄₆O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1186505-18-9
C₂₈H₄₀O

: 762-42-5
dimethyl acetylenedicarboxylate

: 1186505-20-3
C₃₄H₄₆O₅

: 1186505-19-0
C₃₄H₄₆O₅

Guidance literature:: at 110 ℃; for 24h; stereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.06.064

Reference yield:

: 1318052-00-4
C₂₀H₃₄O

: 1186505-20-3
C₃₄H₄₆O₅

Guidance literature:: Multi-step reaction with 6 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.42 h / -60 °C / Inert atmosphere

1.2: 0.17 h / -60 °C / Inert atmosphere

2.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 °C

3.1: pyrrolidine / diethyl ether / 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / 0 °C / Inert atmosphere

4.2: 8 h / 0 - 20 °C / Inert atmosphere

5.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 - 20 °C / Inert atmosphere

5.2: 0 - 35 °C / Inert atmosphere

6.1: 24 h / 110 °C / Inert atmosphere

With pyrrolidine; n-butyllithium; oxalyl dichloride; sodium hydride; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 1.1: Swern oxidation / 1.2: Swern oxidation / 4.2: Wittig reaction / 6.1: Diels-Alder reaction;
DOI:10.1016/j.tet.2011.05.092

Reference yield:

: 1318051-97-6
C₂₁H₃₄O₂

: 1186505-20-3
C₃₄H₄₆O₅

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 6 h / 0 °C

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.42 h / -60 °C / Inert atmosphere

2.2: 0.17 h / -60 °C / Inert atmosphere

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 0 °C

4.1: pyrrolidine / diethyl ether / 20 °C

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.67 h / 0 °C / Inert atmosphere

5.2: 8 h / 0 - 20 °C / Inert atmosphere

6.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 - 20 °C / Inert atmosphere

6.2: 0 - 35 °C / Inert atmosphere

7.1: 24 h / 110 °C / Inert atmosphere

With pyrrolidine; lithium aluminium tetrahydride; n-butyllithium; oxalyl dichloride; sodium hydride; dimethyl sulfoxide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; 2.1: Swern oxidation / 2.2: Swern oxidation / 5.2: Wittig reaction / 7.1: Diels-Alder reaction;
DOI:10.1016/j.tet.2011.05.092