1-{2-[2-{2-[2-(4-methylphenylsulfonyloxy)ethoxy]ethoxy}ethoxy]ethoxy}-4-(triphenylmethyl)benzene

Base Information

Chemical Name:1-{2-[2-{2-[2-(4-methylphenylsulfonyloxy)ethoxy]ethoxy}ethoxy]ethoxy}-4-(triphenylmethyl)benzene
CAS No.:264124-11-0
Molecular Formula:C₄₀H₄₂O₇S
Molecular Weight:666.835
Hs Code.:

Synonyms:1-{2-[2-{2-[2-(4-methylphenylsulfonyloxy)ethoxy]ethoxy}ethoxy]ethoxy}-4-(triphenylmethyl)benzene

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Chemical Property of 1-{2-[2-{2-[2-(4-methylphenylsulfonyloxy)ethoxy]ethoxy}ethoxy]ethoxy}-4-(triphenylmethyl)benzene

Chemical Property:

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Technology Process of 1-{2-[2-{2-[2-(4-methylphenylsulfonyloxy)ethoxy]ethoxy}ethoxy]ethoxy}-4-(triphenylmethyl)benzene

There total 5 articles about 1-{2-[2-{2-[2-(4-methylphenylsulfonyloxy)ethoxy]ethoxy}ethoxy]ethoxy}-4-(triphenylmethyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 98-59-9
p-toluenesulfonyl chloride

: 264124-10-9
1-[2-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethoxy]-4-triphenylmethylbenzene

: 264124-11-0
1-{2-[2-{2-[2-(4-methylphenylsulfonyloxy)ethoxy]ethoxy}ethoxy]ethoxy}-4-(triphenylmethyl)benzene

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 20 ℃; for 5h;
DOI:10.1002/(SICI)1099-0690(200002)2000:4<591::AID-EJOC591>3.0.CO;2-I

Reference yield: 72.0%

: 37860-51-8
tetraethylene glycol di(p-toluenesulfonate)

: 978-86-9
4-tritylphenol

: 264124-11-0
1-{2-[2-{2-[2-(4-methylphenylsulfonyloxy)ethoxy]ethoxy}ethoxy]ethoxy}-4-(triphenylmethyl)benzene

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 1.5h; Heating;
DOI:10.1021/ma034521t

Reference yield:

: 978-86-9
4-tritylphenol

: 264124-11-0
1-{2-[2-{2-[2-(4-methylphenylsulfonyloxy)ethoxy]ethoxy}ethoxy]ethoxy}-4-(triphenylmethyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / K₂CO₃ / dimethylformamide / 2 h / 120 - 130 °C

2: 92 percent / Et₃N; DMAP / CH₂Cl₂ / 5 h / 20 °C

With dmap; potassium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide; 1: Alkylation / 2: Tosylation;
DOI:10.1002/(SICI)1099-0690(200002)2000:4<591::AID-EJOC591>3.0.CO;2-I