1-[2-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethoxy]-4-triphenylmethylbenzene

Base Information

Chemical Name:1-[2-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethoxy]-4-triphenylmethylbenzene
CAS No.:264124-10-9
Molecular Formula:C₃₃H₃₆O₅
Molecular Weight:512.646
Hs Code.:

Synonyms:1-[2-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethoxy]-4-triphenylmethylbenzene

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Chemical Property of 1-[2-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethoxy]-4-triphenylmethylbenzene

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Technology Process of 1-[2-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethoxy]-4-triphenylmethylbenzene

There total 2 articles about 1-[2-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethoxy]-4-triphenylmethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 978-86-9
4-tritylphenol

: 77544-60-6
p-toluenesulfonic acid 2-[2-[2-(2-hydroxyethoxy)ethoxy]ethoxy]ethyl ester

: 264124-10-9
1-[2-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethoxy]-4-triphenylmethylbenzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 120 - 130 ℃; for 2h;
DOI:10.1002/(SICI)1099-0690(200002)2000:4<591::AID-EJOC591>3.0.CO;2-I

Reference yield:

: 112-60-7
Tetraethylene glycol

: 264124-10-9
1-[2-{2-[2-(2-hydroxyethoxy)ethoxy]ethoxy}ethoxy]-4-triphenylmethylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / tetrahydrofuran; water monomer / 6.5 h / 0 °C

2: potassium carbonate / acetonitrile / 24 h / 60 °C

With potassium carbonate; sodium hydroxide; In tetrahydrofuran; water monomer; acetonitrile;
DOI:10.1002/anie.202201882