9-<(1R,2R)-2-benzyloxy-3-<<(tert-butyl)dimethylsilyl>oxy>-1-<<(tert-butyl)dimethylsilyl>oxymethyl>propoxy>adenine

Base Information

• Chemical Name: 9-<(1R,2R)-2-benzyloxy-3-<<(tert-butyl)dimethylsilyl>oxy>-1-<<(tert-butyl)dimethylsilyl>oxymethyl>propoxy>adenine
• CAS No.: 111392-60-0
• Molecular Formula: C₂₉H₄₉N₅O₄Si₂
• Molecular Weight: 587.91

Synonyms:9-<(1R,2R)-2-benzyloxy-3-<<(tert-butyl)dimethylsilyl>oxy>-1-<<(tert-butyl)dimethylsilyl>oxymethyl>propoxy>adenine

Chemical Property of 9-<(1R,2R)-2-benzyloxy-3-<<(tert-butyl)dimethylsilyl>oxy>-1-<<(tert-butyl)dimethylsilyl>oxymethyl>propoxy>adenine

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Technology Process of 9-<(1R,2R)-2-benzyloxy-3-<<(tert-butyl)dimethylsilyl>oxy>-1-<<(tert-butyl)dimethylsilyl>oxymethyl>propoxy>adenine

There total 5 articles about 9-<(1R,2R)-2-benzyloxy-3-<<(tert-butyl)dimethylsilyl>oxy>-1-<<(tert-butyl)dimethylsilyl>oxymethyl>propoxy>adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

tert-butyldimethylsilyl chloride (18162-48-6) + (2R,3R)-2-(6-Amino-purin-9-ylmethoxy)-3-benzyloxy-butane-1,4-diol (111392-57-5) → 9-<(1R,2R)-2-benzyloxy-3-<<(tert-butyl)dimethylsilyl>oxy>-1-<<(tert-butyl)dimethylsilyl>oxymethyl>propoxy>adenine (111392-60-0)

Guidance literature:

With pyridine; silver nitrate; In tetrahydrofuran; at 25 ℃; for 10h;

DOI:10.1002/hlca.19870700127

Reference yield:

N-benzoyladenine (4005-49-6) → 9-<(1R,2R)-2-benzyloxy-3-<<(tert-butyl)dimethylsilyl>oxy>-1-<<(tert-butyl)dimethylsilyl>oxymethyl>propoxy>adenine (111392-60-0)

Guidance literature:

Multi-step reaction with 3 steps

1: Bu₄NI / toluene / Heating

2: NH₃ / methanol / 24 h / 25 °C

3: 96 percent / AgNO₃, pyridine / tetrahydrofuran / 10 h / 25 °C

With pyridine; ammonia; silver nitrate; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; methanol; toluene;

DOI:10.1002/hlca.19870700127

Reference yield:

C26H25ClO6 (111392-42-8) → 9-<(1R,2R)-2-benzyloxy-3-<<(tert-butyl)dimethylsilyl>oxy>-1-<<(tert-butyl)dimethylsilyl>oxymethyl>propoxy>adenine (111392-60-0)

Guidance literature:

Multi-step reaction with 3 steps

1: Bu₄NI / toluene / Heating

2: NH₃ / methanol / 24 h / 25 °C

3: 96 percent / AgNO₃, pyridine / tetrahydrofuran / 10 h / 25 °C

With pyridine; ammonia; silver nitrate; tetra-(n-butyl)ammonium iodide; In tetrahydrofuran; methanol; toluene;

DOI:10.1002/hlca.19870700127

upstream raw materials:

tert-butyldimethylsilyl chloride

(2R,3R)-2-(6-Amino-purin-9-ylmethoxy)-3-benzyloxy-butane-1,4-diol

N-benzoyladenine

C₃₈H₃₃N₅O₇

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