5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione

Base Information

Chemical Name:5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione
CAS No.:1415973-29-3
Molecular Formula:C₂₃H₂₄N₄O₂S
Molecular Weight:420.535
Hs Code.:

Synonyms:5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione

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Technology Process of 5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione

There total 4 articles about 5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₆N₄O₃S

: 1415973-29-3
5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione

Guidance literature:: C₂₃H₂₆N₄O₃S; With sodium methylate; In methanol; for 0.0833333h; Reflux;

With acetic acid; at 20 ℃;
DOI:10.1007/s11172-012-0046-1

Reference yield:

: C₁₅H₂₁N₃O₂

: 1415973-29-3
5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 10 h / 20 °C

2.1: sodium methylate / methanol / 0.08 h / Reflux

2.2: 20 °C

With sodium methylate; In methanol; toluene;
DOI:10.1007/s11172-012-0046-1

Reference yield:

: 38212-30-5
4-(4-methoxyphenyl)piperazine

: 1415973-29-3
5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione

Guidance literature:: Multi-step reaction with 4 steps

1.1: benzene / 3 h / Reflux

2.1: sodium methylate / methanol / 4 h / Reflux

3.1: toluene / 10 h / 20 °C

4.1: sodium methylate / methanol / 0.08 h / Reflux

4.2: 20 °C

With sodium methylate; In methanol; toluene; benzene;
DOI:10.1007/s11172-012-0046-1