5-acetyl-4-methylsulfanyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine

Base Information

Chemical Name:5-acetyl-4-methylsulfanyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine
CAS No.:1415973-22-6
Molecular Formula:C₂₄H₂₆N₄O₂S
Molecular Weight:434.562
Hs Code.:

Synonyms:5-acetyl-4-methylsulfanyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine

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Chemical Property of 5-acetyl-4-methylsulfanyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine

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Technology Process of 5-acetyl-4-methylsulfanyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine

There total 5 articles about 5-acetyl-4-methylsulfanyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1415973-29-3
5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione

: 74-88-4
methyl iodide

: 1415973-22-6
5-acetyl-4-methylsulfanyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine

Guidance literature:: 5-acetyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine-4(3H)-thione; With sodium methylate; In methanol; at 20 ℃; for 0.166667h;

methyl iodide; In methanol; at 20 ℃; for 0.5h;
DOI:10.1007/s11172-012-0046-1

Reference yield:

: C₁₅H₂₁N₃O₂

: 1415973-22-6
5-acetyl-4-methylsulfanyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine

Guidance literature:: Multi-step reaction with 3 steps

1.1: toluene / 10 h / 20 °C

2.1: sodium methylate / methanol / 0.08 h / Reflux

2.2: 20 °C

3.1: sodium methylate / methanol / 0.17 h / 20 °C

3.2: 0.5 h / 20 °C

With sodium methylate; In methanol; toluene;
DOI:10.1007/s11172-012-0046-1

Reference yield:

: C₂₃H₂₆N₄O₃S

: 1415973-22-6
5-acetyl-4-methylsulfanyl-6-[4-(4-methoxyphenyl)piperazin-1-yl]-2-phenylpyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 0.08 h / Reflux

1.2: 20 °C

2.1: sodium methylate / methanol / 0.17 h / 20 °C

2.2: 0.5 h / 20 °C

With sodium methylate; In methanol;
DOI:10.1007/s11172-012-0046-1