bis(4-methoxyphenyl)iodonium fluoride

Base Information

• Chemical Name: bis(4-methoxyphenyl)iodonium fluoride
• CAS No.: 115991-13-4
• Molecular Formula: C₁₄H₁₄IO₂*F
• Molecular Weight: 360.167

Synonyms:bis(4-methoxyphenyl)iodonium fluoride

Chemical Property of bis(4-methoxyphenyl)iodonium fluoride

Chemical Property:

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Technology Process of bis(4-methoxyphenyl)iodonium fluoride

There total 6 articles about bis(4-methoxyphenyl)iodonium fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.2%

bis(4-methoxyphenyl)iodonium trifluoroacetate (457-66-9) → bis(4-methoxyphenyl)iodonium fluoride (115991-13-4)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 1h; Inert atmosphere;

DOI:10.1016/j.jfluchem.2010.04.004

Reference yield:

(2,5-dimethylphenyl)(4'-methoxyphenyl)iodonium hexafluorophosphate → bis(4-methoxyphenyl)iodonium fluoride (115991-13-4) + C15H16IO(1+)*F(1-) + C16H18I(1+)*F(1-)

Guidance literature:

With tetramethylammonium fluoride; In benzene-d6; Darkness;

DOI:10.1016/j.jfluchem.2010.04.004

Reference yield:

(4,5-dimethoxy-2-methylphenyl)-(4'-methoxyphenyl)iodonium hexafluorophosphate → bis(4-methoxyphenyl)iodonium fluoride (115991-13-4) + C16H18IO3(1+)*F(1-) (1224431-52-0) + C18H22IO4(1+)*F(1-)

Guidance literature:

With tetramethylammonium fluoride; In benzene-d6; Darkness;

DOI:10.1016/j.jfluchem.2010.04.004

upstream raw materials:

bis(4-methoxyphenyl)iodonium trifluoroacetate

4-methoxyphenyl (phenyl)iodonium phosphorus hexafluoride

Downstream raw materials:

(4-methoxy-phenyl)-phenyl-iodonium ; fluoride

1-fluoro-4-methoxybenzene

1-fluoro-3-methoxybenzene

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