N-{(Z)-2-Methyl-3-phenyl-1-p-tolyl-3-[(E)-p-tolylimino]-propenyl}-methanesulfonamide

Base Information

Chemical Name:N-{(Z)-2-Methyl-3-phenyl-1-p-tolyl-3-[(E)-p-tolylimino]-propenyl}-methanesulfonamide
CAS No.:126629-95-6
Molecular Formula:C₂₅H₂₆N₂O₂S
Molecular Weight:418.56
Hs Code.:

Synonyms:N-{(Z)-2-Methyl-3-phenyl-1-p-tolyl-3-[(E)-p-tolylimino]-propenyl}-methanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{(Z)-2-Methyl-3-phenyl-1-p-tolyl-3-[(E)-p-tolylimino]-propenyl}-methanesulfonamide

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Technology Process of N-{(Z)-2-Methyl-3-phenyl-1-p-tolyl-3-[(E)-p-tolylimino]-propenyl}-methanesulfonamide

There total 1 articles about N-{(Z)-2-Methyl-3-phenyl-1-p-tolyl-3-[(E)-p-tolylimino]-propenyl}-methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 73305-96-1
N-(3-amino-2-methyl-1-phenyl-3-p-tolyl-allylidene)-4-methyl-aniline

: 124-63-0
methanesulfonyl chloride

: 126629-95-6
N-{(Z)-2-Methyl-3-phenyl-1-p-tolyl-3-[(E)-p-tolylimino]-propenyl}-methanesulfonamide

Guidance literature:: With triethylamine; In dichloromethane; for 12h; Ambient temperature;
DOI:10.1016/S0040-4039(01)80780-2

Reference yield: 87.0%

: 126629-95-6
N-{(Z)-2-Methyl-3-phenyl-1-p-tolyl-3-[(E)-p-tolylimino]-propenyl}-methanesulfonamide

: 126630-01-1
4-Methyl-5-phenyl-3-p-tolyl-2H-[1,2]thiazine 1,1-dioxide

: 106-49-0,12221-03-3
p-toluidine

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; at -78 - 25 ℃; for 12h;
DOI:10.1016/S0040-4039(01)80780-2

Reference yield:

: 126629-95-6
N-{(Z)-2-Methyl-3-phenyl-1-p-tolyl-3-[(E)-p-tolylimino]-propenyl}-methanesulfonamide

: 126974-78-5
2,4-Dimethyl-5-phenyl-3-p-tolyl-2H-[1,2]thiazine 1,1-dioxide

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / lithium diisopropylamide (LDA) / tetrahydrofuran / 12 h / -78 - 25 °C

2: 1.) NaH / 1.) THF, 25 deg C; 2.) THF, 25 deg C, 10 h

With sodium hydride; lithium diisopropyl amide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(01)80780-2