C₂₃H₃₄O₂Si

Base Information

Chemical Name:C₂₃H₃₄O₂Si
CAS No.:1310330-09-6
Molecular Formula:C₂₃H₃₄O₂Si
Molecular Weight:370.607
Hs Code.:

C<sub>23</sub>H<sub>34</sub>O<sub>2</sub>Si

Synonyms:C₂₃H₃₄O₂Si

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Chemical Property of C₂₃H₃₄O₂Si

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Technology Process of C₂₃H₃₄O₂Si

There total 5 articles about C₂₃H₃₄O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1310330-38-1
C₂₅H₃₈O₂Si

: 1310330-09-6
C₂₃H₃₄O₂Si

Guidance literature:: With 1,3-bis-(2,4,6-trimethylphenyl)-2-(imidazolidinylidene)dichloro(5-nitro-2-isopropoxyphenylmethylene)ruthenium; tricyclohexylphosphine oxide; In toluene; at 60 ℃; for 24h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ja2031085

Reference yield:

: C₁₇H₂₄O₂Si

: 1310330-09-6
C₂₃H₃₄O₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: methanol; toluene-4-sulfonic acid / 2 h / Inert atmosphere

2.1: sodium bis(2-methoxyethoxy)aluminium dihydride / diethyl ether; toluene / 2 h / 20 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

3.1: dichloro bis(acetonitrile) palladium(II); Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 1 h / Inert atmosphere

4.1: 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / Inert atmosphere

5.1: 1,3-bis-(2,4,6-trimethylphenyl)-2-(imidazolidinylidene)dichloro(5-nitro-2-isopropoxyphenylmethylene)ruthenium; tricyclohexylphosphine oxide / toluene / 24 h / 60 °C / Inert atmosphere

With methanol; dichloro bis(acetonitrile) palladium(II); 1,3-bis-(2,4,6-trimethylphenyl)-2-(imidazolidinylidene)dichloro(5-nitro-2-isopropoxyphenylmethylene)ruthenium; tricyclohexylphosphine oxide; 4-pyrrolidin-1-ylpyridine; toluene-4-sulfonic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium bis(2-methoxyethoxy)aluminium dihydride; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; In diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja2031085

Reference yield:

: 1310330-35-8
C₁₄H₂₀OSi

: 1310330-09-6
C₂₃H₃₄O₂Si

Guidance literature:: Multi-step reaction with 2 steps

1: 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 1 h / Inert atmosphere

2: 1,3-bis-(2,4,6-trimethylphenyl)-2-(imidazolidinylidene)dichloro(5-nitro-2-isopropoxyphenylmethylene)ruthenium; tricyclohexylphosphine oxide / toluene / 24 h / 60 °C / Inert atmosphere

With 1,3-bis-(2,4,6-trimethylphenyl)-2-(imidazolidinylidene)dichloro(5-nitro-2-isopropoxyphenylmethylene)ruthenium; tricyclohexylphosphine oxide; 4-pyrrolidin-1-ylpyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; toluene;
DOI:10.1021/ja2031085