N₅-(3-chlorophenyl)-N₃-(4-morpholinophenyl)-1,2,4-thiadiazole-3,5-diamine

Base Information

Chemical Name:N₅-(3-chlorophenyl)-N₃-(4-morpholinophenyl)-1,2,4-thiadiazole-3,5-diamine
CAS No.:1421694-74-7
Molecular Formula:C₁₈H₁₈ClN₅OS
Molecular Weight:387.893
Hs Code.:

N<sub>5</sub>-(3-chlorophenyl)-N<sub>3</sub>-(4-morpholinophenyl)-1,2,4-thiadiazole-3,5-diamine

Synonyms:N₅-(3-chlorophenyl)-N₃-(4-morpholinophenyl)-1,2,4-thiadiazole-3,5-diamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N₅-(3-chlorophenyl)-N₃-(4-morpholinophenyl)-1,2,4-thiadiazole-3,5-diamine

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Technology Process of N₅-(3-chlorophenyl)-N₃-(4-morpholinophenyl)-1,2,4-thiadiazole-3,5-diamine

There total 2 articles about N₅-(3-chlorophenyl)-N₃-(4-morpholinophenyl)-1,2,4-thiadiazole-3,5-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2524-67-6,86759-37-7
4-morpholino-4-yl-phenylamine

: 1125866-02-5
C₈H₅Cl₂N₃S

: 1421694-74-7
N₅-(3-chlorophenyl)-N₃-(4-morpholinophenyl)-1,2,4-thiadiazole-3,5-diamine

Guidance literature:: With zinc(II) chloride; at 90 - 120 ℃;
DOI:10.1016/j.tetlet.2012.11.107

Reference yield:

: 108-42-9
3-chloro-aniline

: 1421694-74-7
N₅-(3-chlorophenyl)-N₃-(4-morpholinophenyl)-1,2,4-thiadiazole-3,5-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / cyclohexanol / 20 - 80 °C

2: zinc(II) chloride / 90 - 120 °C

With N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In cyclohexanol;
DOI:10.1016/j.tetlet.2012.11.107