(S)-benzyl 2-((S)-(tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate

Base Information

Chemical Name:(S)-benzyl 2-((S)-(tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate
CAS No.:1192024-61-5
Molecular Formula:C₂₄H₂₈FNO₅
Molecular Weight:429.488
Hs Code.:

Synonyms:(S)-benzyl 2-((S)-(tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate

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Chemical Property of (S)-benzyl 2-((S)-(tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate

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Technology Process of (S)-benzyl 2-((S)-(tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate

There total 2 articles about (S)-benzyl 2-((S)-(tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 139101-19-2
benzyl 2-fluoro-3-oxobutanoate

: 479423-39-7
4-methylbenzaldehyde N-(tert-butoxycarbonyl)imine

: benzyl 2-(tert-butoxycarbonylamino)(p-tolyl)methyl-2-fluoro-3-oxobutanoate

: 1192024-61-5
(S)-benzyl 2-((S)-(tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate

: (R)-benzyl 2-((R)-(tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate

Guidance literature:: With 2BF₄^(1-)*C₄₆H₃₇NOP₂Pd⁽²⁺⁾; In toluene; at 20 ℃; for 10h; optical yield given as %ee; enantioselective reaction;
DOI:10.1016/j.tetlet.2011.02.087

Reference yield:

: 139101-19-2
benzyl 2-fluoro-3-oxobutanoate

: 479423-39-7
4-methylbenzaldehyde N-(tert-butoxycarbonyl)imine

: 1192024-61-5
(S)-benzyl 2-((S)-(tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate

: (R)-benzyl 2-((R)-(tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate

: benzyl 2-((tert-butoxycarbonylamino)(p-tolyl)-methyl)-2-fluoro-3-oxobutanoate

Guidance literature:: With C₃₇H₃₁F₆N₃S; In diethyl ether; at 20 ℃; for 36h; optical yield given as %ee; enantioselective reaction;
DOI:10.5012/bkcs.2011.32.4.1195